(E)-fumaridine

Base Information

Chemical Name:(E)-fumaridine
CAS No.:80299-53-2
Molecular Formula:C₂₂H₂₄N₂O₅
Molecular Weight:396.443
Hs Code.:

Synonyms:

Suppliers and Price of (E)-fumaridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 0 raw suppliers

Chemical Property of (E)-fumaridine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (E)-fumaridine

There total 7 articles about (E)-fumaridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.6%

: 80299-54-3,30341-98-1
fumaridine

: 80299-53-2,30341-98-1
(E)-fumaridine

Guidance literature:: In chloroform; for 6h; Irradiation;
DOI:10.1021/jo00344a025

Reference yield:

: 80299-52-1
α-hydrastine methiodide

: 80299-53-2,30341-98-1
(E)-fumaridine

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / 5percent aq. NaOH / CH₂Cl₂ / 0.17 h / Ambient temperature

2: 47.7 percent / CHCl₃ / 6 h / Irradiation

3: 69 percent / 28percent aq. NH₄OH / acetone / 4 h / Ambient temperature

4: HCl / methanol / 0.17 h / Ambient temperature

5: 32.6 percent / CHCl₃ / 6 h / Irradiation

With hydrogenchloride; ammonium hydroxide; sodium hydroxide; In methanol; dichloromethane; chloroform; acetone;
DOI:10.1021/jo00344a025

Reference yield:

: 51390-68-2
β-hydrastine methiodide

: 80299-53-2,30341-98-1
(E)-fumaridine

Guidance literature:: Multi-step reaction with 5 steps

1: 6 percent / 5percent aq. NaOH / CH₂Cl₂ / 0.17 h / Ambient temperature

2: 47.7 percent / CHCl₃ / 6 h / Irradiation

3: 69 percent / 28percent aq. NH₄OH / acetone / 4 h / Ambient temperature

4: HCl / methanol / 0.17 h / Ambient temperature

5: 32.6 percent / CHCl₃ / 6 h / Irradiation

With hydrogenchloride; ammonium hydroxide; sodium hydroxide; In methanol; dichloromethane; chloroform; acetone;
DOI:10.1021/jo00344a025