(E)-3-(2-Iodo-phenyl)-acryloyl azide

Base Information

Chemical Name:(E)-3-(2-Iodo-phenyl)-acryloyl azide
CAS No.:1027219-61-9
Molecular Formula:C₉H₆IN₃O
Molecular Weight:299.071
Hs Code.:

Synonyms:

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Chemical Property of (E)-3-(2-Iodo-phenyl)-acryloyl azide

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Technology Process of (E)-3-(2-Iodo-phenyl)-acryloyl azide

There total 3 articles about (E)-3-(2-Iodo-phenyl)-acryloyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26260-02-6
2-iodobenzaldehyde

: 1027219-61-9
(E)-3-(2-Iodo-phenyl)-acryloyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / piperidine, pyridine / 1 h / Heating

2: SOCl₂ / dimethylformamide / 16 h

3: NaN₃ / dioxane; H₂O / 0.75 h

With piperidine; pyridine; thionyl chloride; sodium azide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1039/a607202j

Reference yield:

: 5159-41-1
2-iodobenzyl alcohol

: 1027219-61-9
(E)-3-(2-Iodo-phenyl)-acryloyl azide

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / PDC / CH₂Cl₂ / 3 h

2: 82 percent / piperidine, pyridine / 1 h / Heating

3: SOCl₂ / dimethylformamide / 16 h

4: NaN₃ / dioxane; H₂O / 0.75 h

With piperidine; pyridine; dipyridinium dichromate; thionyl chloride; sodium azide; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/a607202j

Reference yield:

: 90276-19-0
(E)-3-(2-Iodophenyl)propenoic acid

: 1027219-61-9
(E)-3-(2-Iodo-phenyl)-acryloyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / dimethylformamide / 16 h

2: NaN₃ / dioxane; H₂O / 0.75 h

With thionyl chloride; sodium azide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1039/a607202j