Technology Process of C20H23NO4
There total 6 articles about C20H23NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
toluene;
at 200 ℃;
for 1h;
Microwave irradiation;
DOI:10.1021/jo501231q
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydroxide / water; dichloromethane / 8 h / 20 °C
2: toluene / 1 h / 200 °C / Microwave irradiation
With
tetra-(n-butyl)ammonium iodide; sodium hydroxide;
In
dichloromethane; water; toluene;
DOI:10.1021/jo501231q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bismuth(III) chloride / acetonitrile; water / 24 h / 0 - 24 °C
2: sodium hydrogencarbonate; sodium periodate / water; dichloromethane / 24 h / 25 °C
3: indium; ammonium chloride / water; tetrahydrofuran / 24 h / 0 °C
4: tetra-(n-butyl)ammonium iodide; sodium hydroxide / water; dichloromethane / 8 h / 20 °C
5: toluene / 1 h / 200 °C / Microwave irradiation
With
bismuth(III) chloride; indium; sodium periodate; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; ammonium chloride; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; toluene; acetonitrile;
3: |Barbier Coupling Reaction;
DOI:10.1021/jo501231q