6-[2-[(E)-(S)-3-(tert-Butyl-dimethyl-silanyloxy)-3-cyclohexyl-propenyl]-5-oxo-3-(tetrahydro-pyran-2-yloxy)-cyclopentylsulfanyl]-hexanoic acid decyl ester

Base Information

Chemical Name:6-[2-[(E)-(S)-3-(tert-Butyl-dimethyl-silanyloxy)-3-cyclohexyl-propenyl]-5-oxo-3-(tetrahydro-pyran-2-yloxy)-cyclopentylsulfanyl]-hexanoic acid decyl ester
CAS No.:83009-68-1
Molecular Formula:C₄₁H₇₄O₆SSi
Molecular Weight:723.186
Hs Code.:

6-[2-[(E)-(S)-3-(tert-Butyl-dimethyl-silanyloxy)-3-cyclohexyl-propenyl]-5-oxo-3-(tetrahydro-pyran-2-yloxy)-cyclopentylsulfanyl]-hexanoic acid decyl ester

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Chemical Property of 6-[2-[(E)-(S)-3-(tert-Butyl-dimethyl-silanyloxy)-3-cyclohexyl-propenyl]-5-oxo-3-(tetrahydro-pyran-2-yloxy)-cyclopentylsulfanyl]-hexanoic acid decyl ester

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Technology Process of 6-[2-[(E)-(S)-3-(tert-Butyl-dimethyl-silanyloxy)-3-cyclohexyl-propenyl]-5-oxo-3-(tetrahydro-pyran-2-yloxy)-cyclopentylsulfanyl]-hexanoic acid decyl ester

There total 5 articles about 6-[2-[(E)-(S)-3-(tert-Butyl-dimethyl-silanyloxy)-3-cyclohexyl-propenyl]-5-oxo-3-(tetrahydro-pyran-2-yloxy)-cyclopentylsulfanyl]-hexanoic acid decyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-Mercapto-hexanoic acid decyl ester

: 83009-68-1,83059-49-8
6-[2-[(E)-(S)-3-(tert-Butyl-dimethyl-silanyloxy)-3-cyclohexyl-propenyl]-5-oxo-3-(tetrahydro-pyran-2-yloxy)-cyclopentylsulfanyl]-hexanoic acid decyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / triethylamine / methanol

2: 1.) 2.0 M tert-BuLi, phenylthiocopper, (Me₂N)3P / 1.) pentane, ether; 2.) pentane, THF, ether

With tert.-butyl lithium; copper(I) thiophenolate; triethylamine; Hexamethylphosphorous triamide; In methanol;
DOI:10.1248/cpb.33.2359

Reference yield:

: 64079-54-5
4-(2-tetrahydropyranyloxy)-2,3-epoxycyclopentan-1-one

: 83009-68-1,83059-49-8
6-[2-[(E)-(S)-3-(tert-Butyl-dimethyl-silanyloxy)-3-cyclohexyl-propenyl]-5-oxo-3-(tetrahydro-pyran-2-yloxy)-cyclopentylsulfanyl]-hexanoic acid decyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / triethylamine / methanol

2: 1.) 2.0 M tert-BuLi, phenylthiocopper, (Me₂N)3P / 1.) pentane, ether; 2.) pentane, THF, ether

With tert.-butyl lithium; copper(I) thiophenolate; triethylamine; Hexamethylphosphorous triamide; In methanol;
DOI:10.1248/cpb.33.2359

Reference yield:

: 71399-48-9
3-cyclohexyl-3RS-hydroxy-1-iodoprop-1E-ene

: 83009-68-1,83059-49-8
6-[2-[(E)-(S)-3-(tert-Butyl-dimethyl-silanyloxy)-3-cyclohexyl-propenyl]-5-oxo-3-(tetrahydro-pyran-2-yloxy)-cyclopentylsulfanyl]-hexanoic acid decyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: 99 percent

3: 1.) 2.0 M tert-BuLi, phenylthiocopper, (Me₂N)3P / 1.) pentane, ether; 2.) pentane, THF, ether

With tert.-butyl lithium; copper(I) thiophenolate; Hexamethylphosphorous triamide;
DOI:10.1248/cpb.33.2359