4-(2-hydroxy-3-isopropylaminopropoxy)phenylglyoxylic acid amide

Base Information

Chemical Name:4-(2-hydroxy-3-isopropylaminopropoxy)phenylglyoxylic acid amide
CAS No.:74908-93-3
Molecular Formula:C₁₄H₂₀N₂O₄
Molecular Weight:280.324
Hs Code.:

Synonyms:

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Chemical Property of 4-(2-hydroxy-3-isopropylaminopropoxy)phenylglyoxylic acid amide

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Technology Process of 4-(2-hydroxy-3-isopropylaminopropoxy)phenylglyoxylic acid amide

There total 4 articles about 4-(2-hydroxy-3-isopropylaminopropoxy)phenylglyoxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68758-68-9
p-hydroxymandelic acid ethyl ester

: 74908-93-3
4-(2-hydroxy-3-isopropylaminopropoxy)phenylglyoxylic acid amide

Guidance literature:: Multi-step reaction with 4 steps

1: CrO₃ / acetic acid; H₂O / 0.5 h / Ambient temperature

2: ccNH₄OH

3: triethylamine / 1 h / 90 °C

4: 0.33 h / 60 - 70 °C

With chromium(VI) oxide; ammonium hydroxide; triethylamine; In water; acetic acid;
DOI:10.1248/cpb.30.196

Reference yield:

: 70080-54-5
4-hydroxy-alpha-oxobenzeneacetic acid ethyl ester

: 74908-93-3
4-(2-hydroxy-3-isopropylaminopropoxy)phenylglyoxylic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1: ccNH₄OH

2: triethylamine / 1 h / 90 °C

3: 0.33 h / 60 - 70 °C

With ammonium hydroxide; triethylamine;
DOI:10.1248/cpb.30.196

Reference yield:

: 81346-69-2
4-hydroxyphenylglyoxylic acid amide

: 74908-93-3
4-(2-hydroxy-3-isopropylaminopropoxy)phenylglyoxylic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1 h / 90 °C

2: 0.33 h / 60 - 70 °C

With triethylamine;
DOI:10.1248/cpb.30.196