(5S,6R)-5,6-Diacetyl-4-methyl-cyclohex-2-enecarboxylic acid 2-oxo-propyl ester

Base Information

• Chemical Name: (5S,6R)-5,6-Diacetyl-4-methyl-cyclohex-2-enecarboxylic acid 2-oxo-propyl ester
• CAS No.: 92656-01-4
• Molecular Formula: C₁₅H₂₀O₅
• Molecular Weight: 280.321
• Mol file: 92656-01-4.mol

Synonyms:

Chemical Property of (5S,6R)-5,6-Diacetyl-4-methyl-cyclohex-2-enecarboxylic acid 2-oxo-propyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (5S,6R)-5,6-Diacetyl-4-methyl-cyclohex-2-enecarboxylic acid 2-oxo-propyl ester

There total 3 articles about (5S,6R)-5,6-Diacetyl-4-methyl-cyclohex-2-enecarboxylic acid 2-oxo-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-hexanedione (110-13-4) → (5S,6R)-5,6-Diacetyl-4-methyl-cyclohex-2-enecarboxylic acid 2-oxo-propyl ester (92656-01-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. SeO₂

2: tetrahydrofuran

With selenium(IV) oxide; In tetrahydrofuran;

DOI:10.1007/BF00904452

Reference yield:

potassium sorbate (24634-61-5,58886-84-3,122093-58-7,590-00-1) → (5S,6R)-5,6-Diacetyl-4-methyl-cyclohex-2-enecarboxylic acid 2-oxo-propyl ester (92656-01-4)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / Heating

2: tetrahydrofuran

In tetrahydrofuran; ethanol;

DOI:10.1007/BF00904452

Reference yield:

(E)-hex-3-ene-2,5-dione (820-69-9) + Sorbinsaeure-(2-oxo-propylester) → (5S,6R)-5,6-Diacetyl-4-methyl-cyclohex-2-enecarboxylic acid 2-oxo-propyl ester (92656-01-4)

Guidance literature:

In tetrahydrofuran;

DOI:10.1007/BF00904452

upstream raw materials:

(E)-hex-3-ene-2,5-dione

2,5-hexanedione

potassium sorbate