(δ-[(3R,4R)-3,4-bis(diphenylphosphino)-1-pyrrolidino]-δ-oxovaleric acid-P,P')(1,5-cyclooctadiene)rhodium-tetrafluoroborate * 1.5 methanol

Base Information

• Chemical Name: (δ-[(3R,4R)-3,4-bis(diphenylphosphino)-1-pyrrolidino]-δ-oxovaleric acid-P,P')(1,5-cyclooctadiene)rhodium-tetrafluoroborate * 1.5 methanol
• CAS No.: 104337-68-0
• Molecular Formula: BF₄*CH₄O*C₄₁H₄₅NO₃P₂Rh
• Molecular Weight: 899.534
• Mol file: 104337-68-0.mol

Synonyms:

Chemical Property of (δ-[(3R,4R)-3,4-bis(diphenylphosphino)-1-pyrrolidino]-δ-oxovaleric acid-P,P')(1,5-cyclooctadiene)rhodium-tetrafluoroborate * 1.5 methanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (δ-[(3R,4R)-3,4-bis(diphenylphosphino)-1-pyrrolidino]-δ-oxovaleric acid-P,P')(1,5-cyclooctadiene)rhodium-tetrafluoroborate * 1.5 methanol

There total 1 articles about (δ-[(3R,4R)-3,4-bis(diphenylphosphino)-1-pyrrolidino]-δ-oxovaleric acid-P,P')(1,5-cyclooctadiene)rhodium-tetrafluoroborate * 1.5 methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate + δ-<(3R,4R)-3,4-Bis(diphenylphophino)pyrrolidino>-δ-oxopentansaeure (104351-44-2) → (δ-[(3R,4R)-3,4-bis(diphenylphosphino)-1-pyrrolidino]-δ-oxovaleric acid-P,P')(1,5-cyclooctadiene)rhodium-tetrafluoroborate * 1.5 methanol (104337-68-0)

Guidance literature:

With methanol; In dichloromethane; (N2), dissolved compounds mixed, stirred for 2 h; volume reduced, CH2Cl2 removed, CH3OH added, precipitated with Et2O, centrifuged, washed with Et2O, dried in vac.; elem. anal.;

upstream raw materials:

δ-<(3R,4R)-3,4-Bis(diphenylphophino)pyrrolidino>-δ-oxopentansaeure