7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin

Base Information

• Chemical Name: 7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin
• CAS No.: 189127-38-6
• Molecular Formula: C₈₀H₁₀₈N₄O₈
• Molecular Weight: 1253.76

Synonyms:

Chemical Property of 7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin

There total 4 articles about 7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[[Pd(1,3-bis(diphenylphosphino)propane)]4(7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin)2][OSO2CF3]8 + tetrabutylammonium trifluoroacetate (39481-22-6) → [Pd(dppp)(CO2CF3)2] (138488-62-7) + 7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin (189127-38-6,853799-75-4)

Guidance literature:

In not given; byproducts: [(C4H9)4N][CF3SO3]; monitored by NMR;

DOI:10.1021/ja0103492

Reference yield:

[[Pt(1,3-bis(diphenylphosphino)propane)]4(7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin)2][OSO2CF3]8 + tetrabutylammonium trifluoroacetate (39481-22-6) → [Pt(1,2-bis(diphenylphosphino)propane)(O2CCF3)2] (360556-95-2) + 7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin (189127-38-6,853799-75-4)

Guidance literature:

In not given; byproducts: [(C4H9)4N][CF3SO3]; monitored by NMR;

DOI:10.1021/ja0103492

Reference yield:

[[Pd(1,3-bis(diphenylphosphino)propane)]4(7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin)2][OSO2CF3]8 + 7,11,15,28-tetracyano-1,21,23,25-tetrakis(2-phenethyl)-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin (360576-40-5) → 4Pd(2+)*2(C6H(CN)(OCH2O)(CHCH2CH2C6H5))4*4(C6H5)2P(CH2)3P(C6H5)2*8SO3CF3(1-)=C252H208F24N8O40P8Pd4S8 + 4Pd(2+)*(C6H(CN)(OCH2O)(CHC11H23))4*(C6H(CN)(OCH2O)(CHCH2CH2C6H5))4*4(C6H5)2P(CH2)3P(C6H5)2*8SO3CF3(1-) + 7,11,15,28-tetracyano-1,21,23,25-tetraundecyl-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin (189127-38-6,853799-75-4)

Guidance literature:

In chloroform-d1; mixed at room temp.; not isolated; monitored by NMR;

DOI:10.1021/ja0103492

upstream raw materials:

7,11,15,28-tetracyano-1,21,23,25-tetrakis(2-phenethyl)-2,20:3,19-dimetheno-1H,21H,23H,25H-bis[1,3]dioxocino[5,4-i:5',4'-i']benzo[1,2-d:5,4-d']-bis[1,3]benzodioxocin

tetrabutylammonium trifluoroacetate

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