9,10-Dimethoxy-N,N-dimethyl-1,2,3,4-tetrahydrobenzisochinolinium-tosylat

Base Information

Chemical Name:9,10-Dimethoxy-N,N-dimethyl-1,2,3,4-tetrahydrobenzisochinolinium-tosylat
CAS No.:93464-60-9
Molecular Formula:C₇H₇O₃S*C₁₇H₂₂NO₂
Molecular Weight:443.564
Hs Code.:

9,10-Dimethoxy-N,N-dimethyl-1,2,3,4-tetrahydrobenz<h>isochinolinium-tosylat

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Chemical Property of 9,10-Dimethoxy-N,N-dimethyl-1,2,3,4-tetrahydrobenzisochinolinium-tosylat

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Technology Process of 9,10-Dimethoxy-N,N-dimethyl-1,2,3,4-tetrahydrobenzisochinolinium-tosylat

There total 3 articles about 9,10-Dimethoxy-N,N-dimethyl-1,2,3,4-tetrahydrobenzisochinolinium-tosylat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 47269-29-4
1,2-Dimethoxy-8-acetonyl-7-(2-dimethylamino-ethyl)-naphthalin

: 93464-60-9
9,10-Dimethoxy-N,N-dimethyl-1,2,3,4-tetrahydrobenzisochinolinium-tosylat

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / hydroxylamine hydrochloride, p-toluenesulfonic acid / toluene / 2 h / Heating

2: 1.) NaOH, p-toluenesulfonyl chloride / 1.) H₂O, acetone, 4 h, 2.) reflux, 4 h

With sodium hydroxide; hydroxylamine hydrochloride; toluene-4-sulfonic acid; p-toluenesulfonyl chloride; In toluene;
DOI:10.1002/ardp.19843171006

Reference yield:

: 93464-57-4
2-(2-Dimethylaminoethyl)-1-(2-hydroxyimino-propyl)-7,8-dimethoxy-naphthalin

: 93464-62-1
2-(2-Dimethylaminoethyl)-1-(hydroxymethyl)-7,8-dimethoxy-naphthalin

: 93464-58-5
1-(Acetylamino-methyl)-2-(2-dimethylaminoethyl)-7,8-dimethoxynaphthalin

: 93464-60-9
9,10-Dimethoxy-N,N-dimethyl-1,2,3,4-tetrahydrobenzisochinolinium-tosylat

Guidance literature:: With sodium hydroxide; p-toluenesulfonyl chloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) H₂O, acetone, 4 h, 2.) reflux, 4 h;
DOI:10.1002/ardp.19843171006

Reference yield:

: 93464-57-4
2-(2-Dimethylaminoethyl)-1-(2-hydroxyimino-propyl)-7,8-dimethoxy-naphthalin

: 98-59-9
p-toluenesulfonyl chloride

: 93464-62-1
2-(2-Dimethylaminoethyl)-1-(hydroxymethyl)-7,8-dimethoxy-naphthalin

: 93464-58-5
1-(Acetylamino-methyl)-2-(2-dimethylaminoethyl)-7,8-dimethoxynaphthalin

: 93464-60-9
9,10-Dimethoxy-N,N-dimethyl-1,2,3,4-tetrahydrobenzisochinolinium-tosylat

Guidance literature:: With sodium hydroxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) H₂O, acetone, 4 h, 2.) reflux, 4 h;
DOI:10.1002/ardp.19843171006