methyl N-tryptophyl-1-benzyltryptophanate hydrochloride

Base Information

Chemical Name:methyl N-tryptophyl-1-benzyltryptophanate hydrochloride
CAS No.:1256796-98-1
Molecular Formula:C₃₀H₃₀N₄O₃*ClH
Molecular Weight:531.054
Hs Code.:

Synonyms:

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Chemical Property of methyl N-tryptophyl-1-benzyltryptophanate hydrochloride

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Technology Process of methyl N-tryptophyl-1-benzyltryptophanate hydrochloride

There total 6 articles about methyl N-tryptophyl-1-benzyltryptophanate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1256796-96-9
methyl N-[N-(tert-butoxycarbonyltryptophyl)]-1-benzyltryptophanate

: 1256796-98-1
methyl N-tryptophyl-1-benzyltryptophanate hydrochloride

Guidance literature:: With hydrogenchloride; acetic acid;
DOI:10.1139/V10-100

Reference yield:

: 1256796-92-5
1-benzyltryptophan hydrochloride

: 1256796-98-1
methyl N-tryptophyl-1-benzyltryptophanate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 0 °C / Reflux

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.17 h / 0 °C

2.2: 0 - 20 °C

3.1: hydrogenchloride; acetic acid

With hydrogenchloride; thionyl chloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1139/V10-100

Reference yield:

: 73-22-3,27732-43-0,80206-30-0,27813-82-7
L-Tryptophan

: 1256796-98-1
methyl N-tryptophyl-1-benzyltryptophanate hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonia; sodium; ferric nitrate / diethyl ether / Cooling with acetone-dry ice; Cooling with ice

2.1: hydrogenchloride / methanol / 20 °C

3.1: thionyl chloride / 0 °C / Reflux

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.17 h / 0 °C

4.2: 0 - 20 °C

5.1: hydrogenchloride; acetic acid

With hydrogenchloride; thionyl chloride; ammonia; sodium; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; ferric nitrate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1139/V10-100