Technology Process of C8H6(2)H2O2
There total 3 articles about C8H6(2)H2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: SOCl2, pyridine / 2 h / 80 °C
2: 62 percent / LiBEt3D / tetrahydrofuran / 16 h
3: 1.) H2SO4, HNO3, 2.) SnCl2, conc. aq. HCl, 3.) K2Cr2O7, aq. H2SO4
With
pyridine; hydrogenchloride; lithium triethyl borodeuteride; potassium dichromate; thionyl chloride; sulfuric acid; nitric acid; tin(ll) chloride;
In
tetrahydrofuran;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 62 percent / LiBEt3D / tetrahydrofuran / 16 h
2: 1.) H2SO4, HNO3, 2.) SnCl2, conc. aq. HCl, 3.) K2Cr2O7, aq. H2SO4
With
hydrogenchloride; lithium triethyl borodeuteride; potassium dichromate; sulfuric acid; nitric acid; tin(ll) chloride;
In
tetrahydrofuran;
- Guidance literature:
-
With
hydrogenchloride; potassium dichromate; sulfuric acid; nitric acid; tin(ll) chloride;