C₃₆H₄₈O₆Si

Base Information

Chemical Name:C₃₆H₄₈O₆Si
CAS No.:1286242-12-3
Molecular Formula:C₃₆H₄₈O₆Si
Molecular Weight:604.859
Hs Code.:

C<sub>36</sub>H<sub>48</sub>O<sub>6</sub>Si

Synonyms:

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Chemical Property of C₃₆H₄₈O₆Si

Chemical Property:

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Technology Process of C₃₆H₄₈O₆Si

There total 15 articles about C₃₆H₄₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1286241-97-1
C₃₀H₄₈O₄Si₂

: 1286242-12-3
C₃₆H₄₈O₆Si

Guidance literature:: Multi-step reaction with 10 steps

1: Dess-Martin periodane / dichloromethane

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

3: trimethylaluminum / dichloromethane; water / -50 °C

4: toluene-4-sulfonic acid / benzene / Reflux

5: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

6: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

7: copper(l) cyanide / diethyl ether / -50 - -30 °C

8: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane

9: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol

10: diethyl ether / 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diethyl (2R,3R)-tartrate; [bis(acetoxy)iodo]benzene; trimethylaluminum; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol; benzene; 1: Dess-Martin oxidation / 1: Wittig reaction / 6: Katsuki-Sharpless epoxidation;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-95-9
C₃₀H₄₈O₃Si₂

: 1286242-12-3
C₃₆H₄₈O₆Si

Guidance literature:: Multi-step reaction with 11 steps

1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

2: Dess-Martin periodane / dichloromethane

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

4: trimethylaluminum / dichloromethane; water / -50 °C

5: toluene-4-sulfonic acid / benzene / Reflux

6: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

7: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

8: copper(l) cyanide / diethyl ether / -50 - -30 °C

9: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane

10: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol

11: diethyl ether / 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diethyl (2R,3R)-tartrate; [bis(acetoxy)iodo]benzene; trimethylaluminum; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol; benzene; 1: Katsuki-Sharpless epoxidation / 2: Dess-Martin oxidation / 2: Wittig reaction / 7: Katsuki-Sharpless epoxidation;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-94-8
C₃₁H₄₈O₄Si₂

: 1286242-12-3
C₃₆H₄₈O₆Si

Guidance literature:: Multi-step reaction with 12 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

3: Dess-Martin periodane / dichloromethane

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

5: trimethylaluminum / dichloromethane; water / -50 °C

6: toluene-4-sulfonic acid / benzene / Reflux

7: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

8: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

9: copper(l) cyanide / diethyl ether / -50 - -30 °C

10: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane

11: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol

12: diethyl ether / 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diethyl (2R,3R)-tartrate; [bis(acetoxy)iodo]benzene; trimethylaluminum; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol; benzene; 2: Katsuki-Sharpless epoxidation / 3: Dess-Martin oxidation / 3: Wittig reaction / 8: Katsuki-Sharpless epoxidation;
DOI:10.3987/COM-10-12106