(E)-3-[4-Hydroxy-3-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylic acid (2R,3S,4S,5R,6S)-3,4,5-trihydroxy-6-[2-hydroxy-4-((E)-2-methoxycarbonyl-vinyl)-phenoxy]-tetrahydro-pyran-2-ylmethyl ester

Base Information

Chemical Name:(E)-3-[4-Hydroxy-3-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylic acid (2R,3S,4S,5R,6S)-3,4,5-trihydroxy-6-[2-hydroxy-4-((E)-2-methoxycarbonyl-vinyl)-phenoxy]-tetrahydro-pyran-2-ylmethyl ester
CAS No.:80596-03-8
Molecular Formula:C₃₁H₃₆O₁₇
Molecular Weight:680.617
Hs Code.:

(E)-3-[4-Hydroxy-3-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylic acid (2R,3S,4S,5R,6S)-3,4,5-trihydroxy-6-[2-hydroxy-4-((E)-2-methoxycarbonyl-vinyl)-phenoxy]-tetrahydro-pyran-2-ylmethyl ester

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Chemical Property of (E)-3-[4-Hydroxy-3-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylic acid (2R,3S,4S,5R,6S)-3,4,5-trihydroxy-6-[2-hydroxy-4-((E)-2-methoxycarbonyl-vinyl)-phenoxy]-tetrahydro-pyran-2-ylmethyl ester

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Technology Process of (E)-3-[4-Hydroxy-3-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylic acid (2R,3S,4S,5R,6S)-3,4,5-trihydroxy-6-[2-hydroxy-4-((E)-2-methoxycarbonyl-vinyl)-phenoxy]-tetrahydro-pyran-2-ylmethyl ester

There total 1 articles about (E)-3-[4-Hydroxy-3-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylic acid (2R,3S,4S,5R,6S)-3,4,5-trihydroxy-6-[2-hydroxy-4-((E)-2-methoxycarbonyl-vinyl)-phenoxy]-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 80596-03-8
(E)-3-[4-Hydroxy-3-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylic acid (2R,3S,4S,5R,6S)-3,4,5-trihydroxy-6-[2-hydroxy-4-((E)-2-methoxycarbonyl-vinyl)-phenoxy]-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: With potassium hydroxide; Yield given. Multistep reaction; 1. hydrolysis at -20 grad C in 75percent aq methanol for 4 h 2. methylation;
DOI:10.1016/S0040-4039(01)81866-9