C₁₅H₂₂O₃

Base Information

Chemical Name:C₁₅H₂₂O₃
CAS No.:951388-84-4
Molecular Formula:C₁₅H₂₂O₃
Molecular Weight:250.338
Hs Code.:

C<sub>15</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₁₅H₂₂O₃

Chemical Property:

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Technology Process of C₁₅H₂₂O₃

There total 4 articles about C₁₅H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 951388-70-8
(2S,5S,6S)-2-(1-hydroxy-2,2-dimethylbut-3-enyl)-5,6-dimethoxy-5,6-dimethyl[1,4]dioxane

: 951388-84-4
C₁₅H₂₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaH / dimethylformamide / 0.5 h / 20 °C

1.2: 68 percent / Bu₄NI / dimethylformamide / 20 °C

2.1: 54 percent / aq. trifluoroacetic acid / CH₂Cl₂ / 0.33 h / 20 °C

3.1: H₂ / Pd/C / 2-methyl-propan-2-ol / 760.05 Torr

4.1: p-toluenesulfonic acid / CH₂Cl₂ / 20 °C

With hydrogen; sodium hydride; toluene-4-sulfonic acid; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.chemphyslip.2006.12.006

Reference yield:

: 951388-81-1
C₂₁H₃₂O₅

: 951388-84-4
C₁₅H₂₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / aq. trifluoroacetic acid / CH₂Cl₂ / 0.33 h / 20 °C

2: H₂ / Pd/C / 2-methyl-propan-2-ol / 760.05 Torr

3: p-toluenesulfonic acid / CH₂Cl₂ / 20 °C

With hydrogen; toluene-4-sulfonic acid; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; tert-butyl alcohol;
DOI:10.1016/j.chemphyslip.2006.12.006

Reference yield:

: 951388-82-2
C₁₅H₂₂O₃

: 951388-84-4
C₁₅H₂₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / 2-methyl-propan-2-ol / 760.05 Torr

2: p-toluenesulfonic acid / CH₂Cl₂ / 20 °C

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In dichloromethane; tert-butyl alcohol;
DOI:10.1016/j.chemphyslip.2006.12.006