12,12,13,13,14,14,15,15,16,16,17,17,17-Tridecafluoro-heptadecanoic acid ((S)-2-benzyloxy-1-hexadecylcarbamoyl-ethyl)-amide

Base Information

Chemical Name:12,12,13,13,14,14,15,15,16,16,17,17,17-Tridecafluoro-heptadecanoic acid ((S)-2-benzyloxy-1-hexadecylcarbamoyl-ethyl)-amide
CAS No.:173439-92-4
Molecular Formula:C₄₃H₆₅F₁₃N₂O₃
Molecular Weight:904.98
Hs Code.:

Synonyms:

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Chemical Property of 12,12,13,13,14,14,15,15,16,16,17,17,17-Tridecafluoro-heptadecanoic acid ((S)-2-benzyloxy-1-hexadecylcarbamoyl-ethyl)-amide

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Technology Process of 12,12,13,13,14,14,15,15,16,16,17,17,17-Tridecafluoro-heptadecanoic acid ((S)-2-benzyloxy-1-hexadecylcarbamoyl-ethyl)-amide

There total 4 articles about 12,12,13,13,14,14,15,15,16,16,17,17,17-Tridecafluoro-heptadecanoic acid ((S)-2-benzyloxy-1-hexadecylcarbamoyl-ethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 118624-66-1
11-(perfluorohexyl)undecanoyl chloride

: 162969-01-9
(S)-2-Amino-3-benzyloxy-N-hexadecyl-propionamide

: 173439-92-4
12,12,13,13,14,14,15,15,16,16,17,17,17-Tridecafluoro-heptadecanoic acid ((S)-2-benzyloxy-1-hexadecylcarbamoyl-ethyl)-amide

Guidance literature:: With triethylamine; for 24h; Ambient temperature;
DOI:10.1016/0040-4020(95)00837-X

Reference yield:

: 143-27-1
hexadecylamine

: 173439-92-4
12,12,13,13,14,14,15,15,16,16,17,17,17-Tridecafluoro-heptadecanoic acid ((S)-2-benzyloxy-1-hexadecylcarbamoyl-ethyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NEt₃, HOBt, DCC / dimethylformamide / 30 min, 0 deg C; 50 deg C, 20 h

2: 100 percent / CF₃COOH / 1 h / Ambient temperature

3: 92 percent / NEt₃ / 24 h / Ambient temperature

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(95)00837-X

Reference yield:

: 23680-31-1
BOC-O-benzyl-L-serine

: 173439-92-4
12,12,13,13,14,14,15,15,16,16,17,17,17-Tridecafluoro-heptadecanoic acid ((S)-2-benzyloxy-1-hexadecylcarbamoyl-ethyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NEt₃, HOBt, DCC / dimethylformamide / 30 min, 0 deg C; 50 deg C, 20 h

2: 100 percent / CF₃COOH / 1 h / Ambient temperature

3: 92 percent / NEt₃ / 24 h / Ambient temperature

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(95)00837-X