trans-3-p-coumaroylquinic acid

Base Information

Chemical Name:trans-3-p-coumaroylquinic acid
CAS No.:82889-89-2
Molecular Formula:C₁₆H₁₈O₈
Molecular Weight:338.314
Hs Code.:

Synonyms:

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Chemical Property of trans-3-p-coumaroylquinic acid

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Technology Process of trans-3-p-coumaroylquinic acid

There total 23 articles about trans-3-p-coumaroylquinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.3%

: 209965-31-1
quinic acid bisacetonide

: 108608-03-3
4-hydroxycinnamic acid chloride

: 1899-30-5,5746-55-4,32451-86-8,32719-13-4,82659-64-1,82659-65-2,82889-89-2,87099-71-6,87099-74-9
trans-3-p-coumaroylquinic acid

Guidance literature:: quinic acid bisacetonide; 4-hydroxycinnamic acid chloride; With pyridine; In dichloromethane;

With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃;

Reference yield: 77.0%

: ethyl 5-O-acetyl-p-coumaroyl-3,4-O-isopropylidenequinate

: 5746-55-4,32451-86-8,32719-13-4,82659-64-1,82659-65-2,82889-89-2,87099-71-6,87099-74-9,1899-30-5
5-O-p-coumaroylquinic acid

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 144h;
DOI:10.1016/j.tetasy.2017.01.015

Reference yield:

: 32384-42-2
(1S,3R,4S,5R)-3,4-O-isopropylidene-1,5-quinic lactone

: 5746-55-4,32451-86-8,32719-13-4,82659-64-1,82659-65-2,82889-89-2,87099-71-6,87099-74-9,1899-30-5
5-O-p-coumaroylquinic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / Inert atmosphere

2: dmap; pyridine / dichloromethane / 24 h / 20 °C

3: hydrogenchloride; water / tetrahydrofuran / 144 h / 20 °C

With pyridine; hydrogenchloride; dmap; water; sodium ethanolate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetasy.2017.01.015