5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzoquinoline

Base Information

Chemical Name:5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzoquinoline
CAS No.:86738-71-8
Molecular Formula:C₂₁H₂₃NO₂
Molecular Weight:321.419
Hs Code.:

5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzo<d,e>quinoline

Synonyms:

Suppliers and Price of 5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzoquinoline

Chemical Property:

Purity/Quality:

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Technology Process of 5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzoquinoline

There total 10 articles about 5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35690-87-0
1,2,3,8,9,9a-hexahydro-5,6-dimethoxy-1-methyl-7H-benzoquinolin-7-one

: 86738-71-8
5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) lithium di-isopropylamide / 1.) THF, hexane, 0.5 h, 2.) 3 h

2: 0.17 g / K, MeOH / 0.5 h / Heating

3: 0.7 g / EtOH / Raney nickel / 0.5 h / Heating

4: 0.1 g / zinc amalgam, HCl / ethanol / 0.67 h / Heating

With hydrogenchloride; methanol; amalgamated zinc; ethanol; lithium diisopropyl amide; nickel; In ethanol;
DOI:10.1039/P19830000909

Reference yield:

: 1483-72-3
diphenyliodonium chloride

: 86738-71-8
5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 0.17 g / K, MeOH / 0.5 h / Heating

2: 0.7 g / EtOH / Raney nickel / 0.5 h / Heating

3: 0.1 g / zinc amalgam, HCl / ethanol / 0.67 h / Heating

With hydrogenchloride; methanol; amalgamated zinc; ethanol; nickel; In ethanol;
DOI:10.1039/P19830000909

Reference yield:

: 345939-41-5
5,6-dimethoxy-1-methyl-8-phenylthio-1,2,3,8,9,9a-hexahydrobenzoquinolin-7-one

: 86738-71-8
5,6-dimethoxy-1-methyl-8-phenyl-2,3,9,9a-tetrahydro-1H-benzoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 0.17 g / K, MeOH / 0.5 h / Heating

2: 0.7 g / EtOH / Raney nickel / 0.5 h / Heating

3: 0.1 g / zinc amalgam, HCl / ethanol / 0.67 h / Heating

With hydrogenchloride; methanol; amalgamated zinc; ethanol; nickel; In ethanol;
DOI:10.1039/P19830000909