(2-{(S)-1-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyl]-3-methyl-butylcarbamoyloxy}-ethyl)-triphenyl-phosphonium

Base Information

Chemical Name:(2-{(S)-1-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyl]-3-methyl-butylcarbamoyloxy}-ethyl)-triphenyl-phosphonium
CAS No.:79134-91-1
Molecular Formula:C₅₂H₆₂N₄O₁₄P
Molecular Weight:998.056
Hs Code.:

(2-{(S)-1-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyl]-3-methyl-butylcarbamoyloxy}-ethyl)-triphenyl-phosphonium

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Chemical Property of (2-{(S)-1-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyl]-3-methyl-butylcarbamoyloxy}-ethyl)-triphenyl-phosphonium

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Technology Process of (2-{(S)-1-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyl]-3-methyl-butylcarbamoyloxy}-ethyl)-triphenyl-phosphonium

There total 4 articles about (2-{(S)-1-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyl]-3-methyl-butylcarbamoyloxy}-ethyl)-triphenyl-phosphonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 73951-87-8
Peoc-Leucin

: 79134-90-0
N⁴-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-asparagin-benzylester

: 79134-91-1
(2-{(S)-1-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyl]-3-methyl-butylcarbamoyloxy}-ethyl)-triphenyl-phosphonium

Guidance literature:: With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane;

Reference yield:

: 4515-24-6
2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosylamine

: 79134-91-1
(2-{(S)-1-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyl]-3-methyl-butylcarbamoyloxy}-ethyl)-triphenyl-phosphonium

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / EEDQ / CHCl₃ / -10 deg C to RT in 12h

2: 67 percent / 20percent HNEt₂ / 2-methyl-propan-2-ol / 0.5 h / Ambient temperature

3: 60 percent / EEDQ / CH₂Cl₂

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; diethylamine; In dichloromethane; chloroform; tert-butyl alcohol;

Reference yield:

: 79134-88-6
{2-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyloxy]-ethyl}-triphenyl-phosphonium

: 79134-91-1
(2-{(S)-1-[(S)-1-Benzyloxycarbonyl-2-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-acetylamino-tetrahydro-pyran-2-ylcarbamoyl)-ethylcarbamoyl]-3-methyl-butylcarbamoyloxy}-ethyl)-triphenyl-phosphonium

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / 20percent HNEt₂ / 2-methyl-propan-2-ol / 0.5 h / Ambient temperature

2: 60 percent / EEDQ / CH₂Cl₂

With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; diethylamine; In dichloromethane; tert-butyl alcohol;