Technology Process of C23H31NO6
There total 4 articles about C23H31NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
5%-palladium/activated carbon; hydrogen;
In
methanol; ethyl acetate;
at 25 ℃;
Inert atmosphere;
DOI:10.1007/s00044-012-0050-x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen bromide; sulfuric acid / dichloromethane / 25 °C
2: potassium carbonate / tetrahydrofuran / 0 - 25 °C
3: 5%-palladium/activated carbon; hydrogen / ethyl acetate; methanol / 25 °C / Inert atmosphere
With
sulfuric acid; 5%-palladium/activated carbon; hydrogen bromide; hydrogen; potassium carbonate;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1007/s00044-012-0050-x
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1,4-diaza-bicyclo[2.2.2]octane / 30 - 40 °C / Sonication
2: hydrogen bromide; sulfuric acid / dichloromethane / 25 °C
3: potassium carbonate / tetrahydrofuran / 0 - 25 °C
4: 5%-palladium/activated carbon; hydrogen / ethyl acetate; methanol / 25 °C / Inert atmosphere
With
1,4-diaza-bicyclo[2.2.2]octane; sulfuric acid; 5%-palladium/activated carbon; hydrogen bromide; hydrogen; potassium carbonate;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
1: |Baylis-Hillman Reaction;
DOI:10.1007/s00044-012-0050-x
