C₂₉H₃₆O₅Si

Base Information

Chemical Name:C₂₉H₃₆O₅Si
CAS No.:945468-54-2
Molecular Formula:C₂₉H₃₆O₅Si
Molecular Weight:492.687
Hs Code.:

C<sub>29</sub>H<sub>36</sub>O<sub>5</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₆O₅Si

Chemical Property:

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Technology Process of C₂₉H₃₆O₅Si

There total 1 articles about C₂₉H₃₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 116996-52-2
(2S)-4-O-(tert-butyldiphenylsilyl)butane-1,2,4-triol

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 945468-54-2
C₂₉H₃₆O₅Si

Guidance literature:: With camphor-10-sulfonic acid; In toluene; for 5h; Heating;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-54-2
C₂₉H₃₆O₅Si

: 945468-56-4
C₃₂H₄₂O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: 71 percent / DIBALH / CH₂Cl₂ / 0.5 h / -78 - 0 °C

2: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 0.25 h / -78 - 0 °C

3: tetrahydrofuran / 0.17 h / -78 °C

4: 90 percent / (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 0.25 h / -78 - 0 °C

5: 71 percent / Zn(BH₄)2 / diethyl ether / 0.33 h / -30 °C

6: VO(acac)2; TBHP / CH₂Cl₂ / 3.5 h / 0 °C

With tert.-butylhydroperoxide; zinc(II) tetrahydroborate; oxalyl dichloride; bis(acetylacetonate)oxovanadium; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; 2: Swern oxidation / 4: Swern oxidation;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-54-2
C₂₉H₃₆O₅Si

: 945468-68-8
C₆₀H₉₆O₁₀Si₄

Guidance literature:: Multi-step reaction with 16 steps

1.1: 71 percent / DIBALH / CH₂Cl₂ / 0.5 h / -78 - 0 °C

2.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 0.25 h / -78 - 0 °C

3.1: tetrahydrofuran / 0.17 h / -78 °C

4.1: 90 percent / (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 0.25 h / -78 - 0 °C

5.1: 71 percent / Zn(BH₄)2 / diethyl ether / 0.33 h / -30 °C

6.1: VO(acac)2; TBHP / CH₂Cl₂ / 3.5 h / 0 °C

7.1: 83 percent / NaH; Bu₄NI / tetrahydrofuran / 2 h / 23 °C

8.1: DDQ / CH₂Cl₂ / 3.5 h / 26 °C / pH 7

9.1: 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

10.1: t-BuLi; Bu₂Mg / tetrahydrofuran / 0.5 h / -20 °C

10.2: 72 percent / tetrahydrofuran / 1 h / 23 °C

11.1: 87 percent / 2,6-lutidine / dimethylformamide / 1.17 h / 0 °C

12.1: 72 percent / Hg(ClO₄)2; 2,6-di-tert-butylpyridine / tetrahydrofuran; H₂O / 0.25 h / 25 °C

13.1: BuLi / tetrahydrofuran / 0.5 h / -78 °C

13.2: 97 percent / tetrahydrofuran / 2 h / -78 °C

14.1: 100 percent / Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 0.08 h / 23 °C

15.1: NaH / benzene; tetrahydrofuran / 0.08 h / 0 °C

15.2: 85 percent / benzene; tetrahydrofuran / 8 h / -78 °C

16.1: 98 percent / NaBH₄; CeCl₃*H₂O / ethanol / 3 h / -20 °C

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; sodium tetrahydroborate; n-butyllithium; 2,6-di-tert-butyl-pyridine; cerium(III) chloride; zinc(II) tetrahydroborate; mercury(II) perchlorate; oxalyl dichloride; bis(acetylacetonate)oxovanadium; dibutylmagnesium; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene; 2.1: Swern oxidation / 4.1: Swern oxidation / 15.1: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetlet.2007.04.136