benzoic acid 17-(acetyl-prop-2-ynyl-amino)-16-hydroxymethyl-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Base Information

• Chemical Name: benzoic acid 17-(acetyl-prop-2-ynyl-amino)-16-hydroxymethyl-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester
• CAS No.: 388564-31-6
• Molecular Formula: C₃₂H₃₉NO₄
• Molecular Weight: 501.666

Synonyms:

Chemical Property of benzoic acid 17-(acetyl-prop-2-ynyl-amino)-16-hydroxymethyl-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of benzoic acid 17-(acetyl-prop-2-ynyl-amino)-16-hydroxymethyl-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

There total 1 articles about benzoic acid 17-(acetyl-prop-2-ynyl-amino)-16-hydroxymethyl-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoic acid 17-(acetyl-prop-2-ynyl-amino)-16-formyl-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester → benzoic acid 17-(acetyl-prop-2-ynyl-amino)-16-hydroxymethyl-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester (388564-31-6)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 - 10 ℃;

DOI:10.1081/SCC-100106037

Reference yield:

benzoic acid 17-(acetyl-prop-2-ynyl-amino)-16-hydroxymethyl-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester (388564-31-6) → benzoic acid 9-iodomethylene-4a,6a-dimethyl-2,3,4,4a,4b,5,6,6a,8,9,12,12a,12b,13-tetradecahydro-1H-10-oxa-7-aza-azuleno[2,1-a]phenanthren-2-yl ester

Guidance literature:

With iodine; sodium hydrogencarbonate; In diethyl ether; water; at 20 ℃; for 3.5h;

DOI:10.1081/SCC-100106037

Reference yield:

benzoic acid 17-(acetyl-prop-2-ynyl-amino)-16-hydroxymethyl-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15-dodecahydro-1H-cyclopenta[a]phenanthren-3-yl ester (388564-31-6) → benzoic acid 4a,6a-dimethyl-9-methylene-2,3,4,4a,4b,5,6,6a,8,9,12,12a,12b,13-tetradecahydro-1H-10-oxa-7-aza-azuleno[2,1-a]phenanthren-2-yl ester

Guidance literature:

Multi-step reaction with 2 steps

1: NaHCO₃; I₂ / H₂O; diethyl ether / 3.5 h / 20 °C

2: 388 mg / aq. Na₂SO₃ / CH₂Cl₂; diethyl ether

With iodine; sodium hydrogencarbonate; sodium sulfite; In diethyl ether; dichloromethane; water;

DOI:10.1081/SCC-100106037

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