Os4(CO)11(μ4-η2-CHCC(CH3)2NHCOC6H9)

Base Information

• Chemical Name: Os4(CO)11(μ4-η2-CHCC(CH3)2NHCOC6H9)
• CAS No.: 126823-27-6
• Molecular Formula: C₂₃H₁₇NO₁₂Os₄
• Molecular Weight: 1260.19
• Mol file: 126823-27-6.mol

Synonyms:

Chemical Property of Os4(CO)11(μ4-η2-CHCC(CH3)2NHCOC6H9)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Os4(CO)11(μ4-η2-CHCC(CH3)2NHCOC6H9)

There total 1 articles about Os4(CO)11(μ4-η2-CHCC(CH3)2NHCOC6H9) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

dodecacarbonyl triosmium (15696-40-9) + N-(α,α-dimethylpropargyl)-1-cyclohexenecarboxamide (126823-21-0) → Os4(CO)11(μ4-η2-CHCC(CH3)2NHCOC6H9) (126823-27-6) + (μ-H)Os3(CO)9(μ3-η2-CCCMe2NHCOC6H9) (126823-26-5)

Guidance literature:

In toluene; (dry N2); refluxing Ru-compd. and org. compd. in dry toluene (25 min); TLC (SiO2, light petroleum/Et2O 50:50); elem. anal.;

upstream raw materials:

dodecacarbonyl triosmium

N-(α,α-dimethylpropargyl)-1-cyclohexenecarboxamide

Refernces