C₄₃H₄₅N₇O₅

Base Information

Chemical Name:C₄₃H₄₅N₇O₅
CAS No.:1402855-89-3
Molecular Formula:C₄₃H₄₅N₇O₅
Molecular Weight:739.874
Hs Code.:

C<sub>43</sub>H<sub>45</sub>N<sub>7</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₃H₄₅N₇O₅

Chemical Property:

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Technology Process of C₄₃H₄₅N₇O₅

There total 4 articles about C₄₃H₄₅N₇O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402855-87-1
C₄₃H₄₇N₇O₆

: 1402855-89-3
C₄₃H₄₅N₇O₅

Guidance literature:: With triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;
DOI:10.1002/psc.2442

Reference yield:

: 1402855-85-9
C₂₁H₂₆N₂O₅

: 1402855-89-3
C₄₃H₄₅N₇O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 3 h / 0 - 20 °C

1.2: 2 h / 0 - 20 °C

1.3: 12 h / 0 - 20 °C

2.1: triethylamine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12.5 h / -20 - 0 °C

3.1: triethylamine; trifluoroacetic anhydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.08 h / 0 °C

With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/psc.2442

Reference yield:

: 1822-51-1
4-picolylchloride hydrochloride

: 1402855-89-3
C₄₃H₄₅N₇O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 20 °C

2.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 3 h / 0 - 20 °C

2.2: 2 h / 0 - 20 °C

2.3: 12 h / 0 - 20 °C

3.1: triethylamine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12.5 h / -20 - 0 °C

4.1: triethylamine; trifluoroacetic anhydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.08 h / 0 °C

With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic anhydride; potassium iodide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/psc.2442