C₂₅H₂₃N₅O₂

Base Information

Chemical Name:C₂₅H₂₃N₅O₂
CAS No.:1550179-88-8
Molecular Formula:C₂₅H₂₃N₅O₂
Molecular Weight:425.49
Hs Code.:

C<sub>25</sub>H<sub>23</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₃N₅O₂

Chemical Property:

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Technology Process of C₂₅H₂₃N₅O₂

There total 5 articles about C₂₅H₂₃N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₁₄N₄O₂

: 81863-45-8
3-(hydroxymethyl)-6-methylaniline

: 1550179-88-8
C₂₅H₂₃N₅O₂

Guidance literature:: With 2-( 1H-7-azabenzotniazol-1-yl)-1,1,3,3-tetrarmethyluroniumhexafluorophosphate methanaminium; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 85 ℃;
DOI:10.1016/j.bmcl.2013.12.050

Reference yield:

: 1780-31-0
2,6-dichloro-5-methylpyrimidine

: 1550179-88-8
C₂₅H₂₃N₅O₂

Guidance literature:: Multi-step reaction with 4 steps

1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide; water / 80 °C

2: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / 1,4-dioxane / 3 h / 170 °C / Microwave irradiation

3: sodium hydroxide; water / methanol / Reflux

4: 2-( 1H-7-azabenzotniazol-1-yl)-1,1,3,3-tetrarmethyluroniumhexafluorophosphate methanaminium; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 85 °C

With bis-triphenylphosphine-palladium(II) chloride; 2-( 1H-7-azabenzotniazol-1-yl)-1,1,3,3-tetrarmethyluroniumhexafluorophosphate methanaminium; water; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; 1: |Suzuki Coupling / 2: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.bmcl.2013.12.050

Reference yield:

: C₁₈H₁₆N₄O₂

: 1550179-88-8
C₂₅H₂₃N₅O₂

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / methanol / Reflux

2: 2-( 1H-7-azabenzotniazol-1-yl)-1,1,3,3-tetrarmethyluroniumhexafluorophosphate methanaminium; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 85 °C

With 2-( 1H-7-azabenzotniazol-1-yl)-1,1,3,3-tetrarmethyluroniumhexafluorophosphate methanaminium; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.12.050