2,4-dinitrophenyl phenyl sulphoxide

Base Information

• Chemical Name: 2,4-dinitrophenyl phenyl sulphoxide
• CAS No.: 69632-18-4
• Molecular Formula: C₁₂H₈N₂O₅S
• Molecular Weight: 292.272
• Mol file: 69632-18-4.mol

Synonyms:

Chemical Property of 2,4-dinitrophenyl phenyl sulphoxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-dinitrophenyl phenyl sulphoxide

There total 5 articles about 2,4-dinitrophenyl phenyl sulphoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2,4-dinitro-1-phenylsulfanyl-benzene (2486-09-1) → 2,4-dinitrophenyl phenyl sulphoxide (19093-39-1,69632-17-3,69632-18-4)

Guidance literature:

With dihydrogen peroxide; In acetic acid; at 50 ℃; for 4h;

Reference yield: 82.0%

2-(phenylthio)ethanol (699-12-7) → 2,4-dinitrophenyl phenyl sulphoxide (19093-39-1,69632-17-3,69632-18-4)

Guidance literature:

With nicotinic acid hydrobromide perbromide; In tetrahydrofuran; water; at 20 ℃; for 2h;

DOI:10.1080/10426500701670683

Reference yield:

1-chloro-2,4-dinitro-benzene (97-00-7) → 2,4-dinitrophenyl phenyl sulphoxide (19093-39-1,69632-17-3,69632-18-4)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol; water

2: 3-chloro-benzenecarboperoxoic acid

With 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In ethanol; water;

DOI:10.1021/cb500789h

upstream raw materials:

2,4-dinitro-1-phenylsulfanyl-benzene

2-(phenylthio)ethanol

thiophenol

1-chloro-2,4-dinitro-benzene

Downstream raw materials:

1-(2,4-dinitrophenyl)piperidine

potassium 2,4-dinitrophenolate