dimethyl (5-trans-2-methoxytetrahydropyranyl)sulphonium toluene-p-sulphonate

Base Information

Chemical Name:dimethyl (5-trans-2-methoxytetrahydropyranyl)sulphonium toluene-p-sulphonate
CAS No.:120466-95-7
Molecular Formula:C₇H₇O₃S*C₈H₁₇O₂S
Molecular Weight:348.485
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl (5-trans-2-methoxytetrahydropyranyl)sulphonium toluene-p-sulphonate

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Technology Process of dimethyl (5-trans-2-methoxytetrahydropyranyl)sulphonium toluene-p-sulphonate

There total 2 articles about dimethyl (5-trans-2-methoxytetrahydropyranyl)sulphonium toluene-p-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 120466-91-3,120466-96-8
trans-2-methoxy-5-methylsulphenyltetrahydropyran

: 80-48-8
methyl p-toluene sulfonate

: 120466-95-7
dimethyl (5-trans-2-methoxytetrahydropyranyl)sulphonium toluene-p-sulphonate

Guidance literature:: at 30 ℃; for 8h;
DOI:10.1039/P29880001225

Reference yield:

: 2-methoxy-5-S-thioacetyltetrahydropyran

: 120466-95-7
dimethyl (5-trans-2-methoxytetrahydropyranyl)sulphonium toluene-p-sulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) aq. 20 percent KOH / 1.) methanol, 1 h, reflux; 2.) reflux, 30 min, methanol

2: 75 percent / 8 h / 30 °C

With potassium hydroxide;
DOI:10.1039/P29880001225