C₂₁H₁₅Cl₂N₃O₃

Base Information

Chemical Name:C₂₁H₁₅Cl₂N₃O₃
CAS No.:701251-10-7
Molecular Formula:C₂₁H₁₅Cl₂N₃O₃
Molecular Weight:428.274
Hs Code.:

C<sub>21</sub>H<sub>15</sub>Cl<sub>2</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₁H₁₅Cl₂N₃O₃

Chemical Property:

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Technology Process of C₂₁H₁₅Cl₂N₃O₃

There total 6 articles about C₂₁H₁₅Cl₂N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-57-0
2-hydroxy-5-nitroaniline

: 701251-10-7
C₂₁H₁₅Cl₂N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: oxygen; pyrographite / 5,5-dimethyl-1,3-cyclohexadiene / 4 h / 120 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 6 h / 20 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; oxygen; pyrographite; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; 5,5-dimethyl-1,3-cyclohexadiene; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm400241j

Reference yield:

: 66423-06-1,66768-02-3,58048-39-8
ethyl 2-(2,4-dichlorophenoxy)propionate

: 701251-10-7
C₂₁H₁₅Cl₂N₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / tetrahydrofuran / 3 h / 80 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

With water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm400241j

Reference yield:

: 120-83-2,40477-79-0
2,4-dichlorophenol

: 701251-10-7
C₂₁H₁₅Cl₂N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

2: water; sodium hydroxide / tetrahydrofuran / 3 h / 80 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

With water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm400241j