Di-Mu-chlorobis[2-[(diMethylaMino)Methyl]-4,6-diMethoxyphenyl-C,N]dipalladiuM(II)

Base Information

• Chemical Name: Di-Mu-chlorobis[2-[(diMethylaMino)Methyl]-4,6-diMethoxyphenyl-C,N]dipalladiuM(II)
• CAS No.: 18987-71-8
• Molecular Formula: C₂₂H₃₂Cl₂N₂O₄Pd₂
• Molecular Weight: 672.253

Synonyms:

Chemical Property of Di-Mu-chlorobis[2-[(diMethylaMino)Methyl]-4,6-diMethoxyphenyl-C,N]dipalladiuM(II)

Chemical Property:

• Melting Point: 180°C(lit.)

Purity/Quality:

97% ^*data from raw suppliers

Di-mu-chlorobis[2-[(dimethylamino)methyl]-4,6-dimethoxyphenyl-C,N]dipalladium(II) >98.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Di-Mu-chlorobis[2-[(diMethylaMino)Methyl]-4,6-diMethoxyphenyl-C,N]dipalladiuM(II)

There total 1 articles about Di-Mu-chlorobis[2-[(diMethylaMino)Methyl]-4,6-diMethoxyphenyl-C,N]dipalladiuM(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

lithium tetrachloropalladate + 3,5-bis(methoxy)-N,N-dimethylbenzylamine (39727-93-0) → di-μ-chlorobis(N,N-dimethyl-3,5-dimethoxybenzylamine-2,C,N)dipalladium(II) (18987-71-8,85440-09-1)

Guidance literature:

In methanol; soln. of benzylamine in MeOH treated with soln. of Li2PdCl4 in MeOH, kept for 24 h at 24-33 °C; ppt. sepd., washed with MeOH, dried at room temp., dissolved in hot CHCl3, filtered through column of Celite, filtrate crystd. from CHCl3 or CHCl3/MeOH; elem. anal.;

DOI:10.1016/0022-328X(83)89535-7

Reference yield:

di-μ-chlorobis(N,N-dimethyl-3,5-dimethoxybenzylamine-2,C,N)dipalladium(II) (18987-71-8,85440-09-1) → chloro(N,N-dimethyl-3,5-dimethoxybenzylamine-2,C,N)(triphenylphosphine)palladium(II) (85380-27-4)

Guidance literature:

With triphenylphosphine; In dichloromethane; kept for 30 min; filtered through Celite, Celite washed with CH2Cl2, to combined CH2Cl2 solns. added hexane, ppt. sepd., crystd. from hot CH2Cl2/hexane; elem. anal.;

DOI:10.1016/0022-328X(83)89535-7

upstream raw materials:

3,5-bis(methoxy)-N,N-dimethylbenzylamine

Downstream raw materials:

chloro(N,N-dimethyl-3,5-dimethoxybenzylamine-2,C,N)(triphenylphosphine)palladium(II)

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