C₆H₆Ru(PMe₃)(PPh₃)

Base Information

Chemical Name:C₆H₆Ru(PMe₃)(PPh₃)
CAS No.:84664-22-2
Molecular Formula:C₂₇H₃₀P₂Ru
Molecular Weight:517.553
Hs Code.:

C<sub>6</sub>H<sub>6</sub>Ru(PMe<sub>3</sub>)(PPh<sub>3</sub>)

Synonyms:

Suppliers and Price of C₆H₆Ru(PMe₃)(PPh₃)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₆H₆Ru(PMe₃)(PPh₃)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of C₆H₆Ru(PMe₃)(PPh₃)

There total 1 articles about C₆H₆Ru(PMe₃)(PPh₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78343-15-4
[C₆H₆RuCl(P(CH₃)3)(P(C₆H₅)3)]⁽¹⁺⁾*PF₆^(1-) = [C₆H₆RuCl(P(CH₃)3)(P(C₆H₅)3)]PF₆

: 84664-22-2
C₆H₆Ru(PMe₃)(PPh₃)

Guidance literature:: With NaC₁₀H₈; In tetrahydrofuran; byproducts: naphthalene, NaCl, NaPF6; under N2, -78°C; hexane was added to the soln. and stirred for 5 min at -78°C, then filtered and the filtrate was dried, the product was dissolved in pentane, filtered and evapd.;

Reference yield:

: ammonium hexafluorophosphate

: 84664-22-2
C₆H₆Ru(PMe₃)(PPh₃)

: 84664-50-6
(Benzol)methyl(trimethylphosphan)(triphenylphosphan)ruthenium(II)-hexafluorophosphat

Guidance literature:: With methyl iodide; In tetrahydrofuran; methanol; byproducts: NH4I; CH3I was slowly added to the complex compd. in THF at -78°C under N2 then stirred at room temp. for 5 min, after pptn. by ether, the soln. was decanted, washed with ether, then NH4PF6 in methanol was added tothe dried intermediate; the product was washed with ether, dried in vac., recrystd. from acetone/ether; elem. anal.;

Reference yield:

: ammonium hexafluorophosphate

: 84664-22-2
C₆H₆Ru(PMe₃)(PPh₃)

: 84664-34-6
(Benzol)hydrido(trimethylphosphan)(triphenylphosphan)ruthenium(II)-hexafluorophosphat

Guidance literature:: In methanol; diethyl ether; byproducts: NH3; under N2, the soln. of ArM(PR3)2 was dried in vac. at -20°C, theresidue was dissolved in ether and cooled to -78°C, NH4PF6 in methanol was added; after warming up to room temp. the soln. was decanted, the ppt. was washed with methanol/ether and with ether, dried in vac., recrystd. from acetone/ether; elem. anal.;