tert-butyl(phenylethynyl)mercury

Base Information

Chemical Name:tert-butyl(phenylethynyl)mercury
CAS No.:108230-30-4
Molecular Formula:C₁₂H₁₄Hg
Molecular Weight:358.833
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl(phenylethynyl)mercury

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Technology Process of tert-butyl(phenylethynyl)mercury

There total 1 articles about tert-butyl(phenylethynyl)mercury which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38442-51-2
tert-butylmercury chloride

: 536-74-3
phenylacetylene

: 108230-30-4
tert-butyl(phenylethynyl)mercury

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; n-BuLi in hexane is added dropwise to PhCCH (THF, ice bath, N2), stirring for a few minutes, warming to room temp. for 5 min, t-BuHgCl is added (ice-bath, mixt. back-flushed with N2), stirring at room temp. for 15 min; mixt. poured into H2O, extd. with ether, washed twice with water, dried over anhydrous Na2SO4, evapd.;
DOI:10.1021/om00093a020

Reference yield: 56.0%

: 108230-30-4
tert-butyl(phenylethynyl)mercury

: 6077-10-7
bis(phenylethynyl)mercury

: mercury

Guidance literature:: In benzene; Irradiation (UV/VIS); symmetrization reaction of substrate in nitrogen-purged solvent in Pyrex tube with 350-nm Rayonet photoreactor for 24 h; GLC; Kinetics;
DOI:10.1021/om00093a020