(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OH)2

Base Information

Chemical Name:(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OH)2
CAS No.:1185739-17-6
Molecular Formula:C₄₀H₇₂GeN₄O₂
Molecular Weight:713.627
Hs Code.:

(2,6-[CH<sub>2</sub>N(iPr)2]2C<sub>6</sub>H<sub>3</sub>)2Ge(OH)2

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Chemical Property of (2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OH)2

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Technology Process of (2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OH)2

There total 7 articles about (2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OH)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1185739-14-3
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(F)OH

: 7732-18-5
water

: 594-19-4
tert.-butyl lithium

: 1185739-17-6
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OH)2

Guidance literature:: In diethyl ether; under inert atm. soln. t-BuLi in pentane was added at 0°C to soln. Ge complex in Et2O, warmed to room temp., H2O was added and stirred for 30 min; solvent was removed in vacuo, pentane was added, ppt. was filtered; elem. anal.;
DOI:10.1002/ejic.200800494

Reference yield: 30.0%

: 1185739-13-2
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OMe)2

: 7732-18-5
water

: 1185739-17-6
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OH)2

Guidance literature:: With Bu₄NF; In tetrahydrofuran; toluene; under inert atm. soln. Ge complex and Bu4NF in THF containing H2O in toluene was heated at reflux for 3 h; solvent was removed in vacuo, residue was solubilized in pentane and crystd. at -20°C; elem. anal.;
DOI:10.1002/ejic.200800494

Reference yield:

: 2,6-bis(diisopropylaminomethyl)phenyllithium

: 1185739-17-6
(2,6-[CH₂N(iPr)2]2C₆H₃)2Ge(OH)2

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: Bu₄NF / tetrahydrofuran; toluene

With Bu₄NF; In tetrahydrofuran; toluene;
DOI:10.1002/ejic.200800494