4,7-Methano-1H-isoindole,2,3,3a,4,7,7a-hexahydro-2-[3-(4-morpholinyl)propyl]-

Base Information

• Chemical Name: 4,7-Methano-1H-isoindole,2,3,3a,4,7,7a-hexahydro-2-[3-(4-morpholinyl)propyl]-
• CAS No.: 73855-76-2
• Molecular Formula: C₁₆H₂₆N₂O
• Molecular Weight: 262.395
• Mol file: 73855-76-2.mol

Synonyms:4,7-Methanoisoindoline,3a,4,7,7a-tetrahydro-2-(3-morpholinopropyl)- (6CI,7CI)

Chemical Property of 4,7-Methano-1H-isoindole,2,3,3a,4,7,7a-hexahydro-2-[3-(4-morpholinyl)propyl]-

Chemical Property:

• Vapor Pressure: 5.62E-06mmHg at 25°C
• Boiling Point: 380°C at 760 mmHg
• Flash Point: 111.3°C
• PSA: 15.71000
• Density: 1.082g/cm³
• LogP: 1.33840

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,7-Methano-1H-isoindole,2,3,3a,4,7,7a-hexahydro-2-[3-(4-morpholinyl)propyl]-

There total 4 articles about 4,7-Methano-1H-isoindole,2,3,3a,4,7,7a-hexahydro-2-[3-(4-morpholinyl)propyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(3-morpholino-propyl)-(3ac,7ac)-3a,4,7,7a-tetrahydro-4r,7c-methano-isoindole-1,3-dione (74039-16-0) → 2-(3-morpholino-propyl)-(3ar,7ac)-2,3,3a,4,7,7a-hexahydro-1H-4r,7c-methano-isoindole (73855-76-2)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

DOI:10.1021/ja01116a010

Reference yield:

4-(3-Aminopropyl)morpholine (123-00-2) → 2-(3-morpholino-propyl)-(3ar,7ac)-2,3,3a,4,7,7a-hexahydro-1H-4r,7c-methano-isoindole (73855-76-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Erhitzen des Reaktionsprodukts auf 170grad

2: LiAlH₄; diethyl ether

With lithium aluminium tetrahydride; diethyl ether;

DOI:10.1021/ja01116a010

Reference yield:

3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride (129-64-6) → 2-(3-morpholino-propyl)-(3ar,7ac)-2,3,3a,4,7,7a-hexahydro-1H-4r,7c-methano-isoindole (73855-76-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Erhitzen des Reaktionsprodukts auf 170grad

2: LiAlH₄; diethyl ether

With lithium aluminium tetrahydride; diethyl ether;

DOI:10.1021/ja01116a010

upstream raw materials:

2-(3-morpholino-propyl)-(3ac,7ac)-3a,4,7,7a-tetrahydro-4r,7c-methano-isoindole-1,3-dione

4-(3-Aminopropyl)morpholine

3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride

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