5,15-bis(2-carboxyphenyl)etioporphyrin II

Base Information

Chemical Name:5,15-bis(2-carboxyphenyl)etioporphyrin II
CAS No.:150994-05-1
Molecular Formula:C₄₆H₄₆N₄O₄
Molecular Weight:718.896
Hs Code.:

Synonyms:

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Chemical Property of 5,15-bis(2-carboxyphenyl)etioporphyrin II

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Technology Process of 5,15-bis(2-carboxyphenyl)etioporphyrin II

There total 3 articles about 5,15-bis(2-carboxyphenyl)etioporphyrin II which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 131531-52-7,151063-01-3,151063-03-5
5,15-Bis(2-(methoxycarbonyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphine

: 150994-05-1,151063-04-6
5,15-bis(2-carboxyphenyl)etioporphyrin II

Guidance literature:: With potassium hydroxide; In pyridine; methanol; water; for 72h; Heating; in the dark;
DOI:10.1246/bcsj.63.2672

Reference yield:

: 92415-30-0
bis(3-ethyl-4-methyl-1H-pyrrol-2-yl)methane

: 150994-05-1,151063-04-6
5,15-bis(2-carboxyphenyl)etioporphyrin II

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / trichloroacetic acid, chloranil / acetonitrile; tetrahydrofuran / 5 h / Ambient temperature

2: 71 percent / potassium hydroxide / pyridine; H₂O; methanol / 72 h / Heating; in the dark

With potassium hydroxide; chloranil; trichloroacetic acid; In tetrahydrofuran; pyridine; methanol; water; acetonitrile;
DOI:10.1246/bcsj.63.2672

Reference yield:

: 4122-56-9
methyl o-formylbenzoate

: 150994-05-1,151063-04-6
5,15-bis(2-carboxyphenyl)etioporphyrin II

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / trichloroacetic acid, chloranil / acetonitrile; tetrahydrofuran / 5 h / Ambient temperature

2: 71 percent / potassium hydroxide / pyridine; H₂O; methanol / 72 h / Heating; in the dark

With potassium hydroxide; chloranil; trichloroacetic acid; In tetrahydrofuran; pyridine; methanol; water; acetonitrile;
DOI:10.1246/bcsj.63.2672