(p-CH₃C₆H₄)3GeCH(p-CH₃C₆H₄)CH₂COOH

Base Information

Chemical Name:(p-CH₃C₆H₄)3GeCH(p-CH₃C₆H₄)CH₂COOH
CAS No.:146139-14-2
Molecular Formula:C₃₁H₃₂GeO₂
Molecular Weight:509.184
Hs Code.:

(p-CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>)3GeCH(p-CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>)CH<sub>2</sub>COOH

Synonyms:

Suppliers and Price of (p-CH₃C₆H₄)3GeCH(p-CH₃C₆H₄)CH₂COOH

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (p-CH₃C₆H₄)3GeCH(p-CH₃C₆H₄)CH₂COOH

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of (p-CH₃C₆H₄)3GeCH(p-CH₃C₆H₄)CH₂COOH

There total 1 articles about (p-CH₃C₆H₄)3GeCH(p-CH₃C₆H₄)CH₂COOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136026-03-4
Cl₃GeCH(C₆H₄CH₃)CH₂COOH

: 4294-57-9
para-methylphenylmagnesium bromide

: 146139-14-2
(p-CH₃C₆H₄)3GeCH(p-CH₃C₆H₄)CH₂COOH

Guidance literature:: In tetrahydrofuran; Mg-compd. added dropwise at 0°C to Ge-compd. in THF, refluxed for4 h, cooled; 10% aq. HCl added, extracted with CHCl3, CHCl3 phase dried over anhydrous MgSO4, filtered, solv. removed in vac., recrystallised from CHCl3 and acetone (3:1);
DOI:10.1080/15533170701301470

Reference yield: 98.0%

: 146139-14-2
(p-CH₃C₆H₄)3GeCH(p-CH₃C₆H₄)CH₂COOH

: 13356-08-6,12684-28-5
fenbutatin oxide

: 341511-30-6
(CH₃C₆H₄)3GeCH(C₆H₄CH₃)CH₂COOSn(CH₂C(CH₃)2C₆H₅)3

Guidance literature:: In toluene; byproducts: H2O; refluxing a mixt of germanium and tin compds. in toluene for 6 h with a Dean-Stark apparatus, cooling; evapn., drying in vac., recrystn. (CHCl3/petroleum ether); elem. anal.;
DOI:10.1016/S0022-328X(00)00542-8

Reference yield: 81.0%

: 146139-14-2
(p-CH₃C₆H₄)3GeCH(p-CH₃C₆H₄)CH₂COOH

: 3682-12-0
diethyltin(IV) oxide

: bis[3-(tri-p-tolylgermyl)-3-p-tolylpropionato]diethyltin(IV)

Guidance literature:: In toluene; Ge-compound and diethyltin oxide added to toluene, refluxed for 8-9 h; water removed, cooled to room temp., toluene removed under reduced pressure, recrystd. from chloroform/n-hexane; elem. anal.;
DOI:10.1016/j.jorganchem.2005.12.013