{PdCl(TeC₆H₄OCH₃-4)}

Base Information

Chemical Name:{PdCl(TeC₆H₄OCH₃-4)}
CAS No.:119053-80-4
Molecular Formula:C₇H₇OTe*Cl*Pd
Molecular Weight:376.605
Hs Code.:

{PdCl(TeC<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>-4)}

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {PdCl(TeC₆H₄OCH₃-4)}

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Technology Process of {PdCl(TeC₆H₄OCH₃-4)}

There total 2 articles about {PdCl(TeC₆H₄OCH₃-4)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 16940-66-2
sodium tetrahydroborate

: sodium tetrachloropalladate(II)

: 35684-37-8
bis(4-methoxyphenyl)ditelluride

: 119053-80-4
{PdCl(TeC₆H₄OCH₃-4)}

Guidance literature:: In ethanol; under N2, molar educt ratio Te2Ar2:Na2(PdCl4) =1:2, dropwise addn. of an ethanolic soln. of NaBH4 to Te2(C6H4OCH3-4)2 in ethanol at room temp. under stirring, addn. of Na2(PdCl4) in ethanol, stirred for 4 h; filtered, washed with water, ethanol and ether, dried in vac.; elem. anal.;
DOI:10.1016/S0020-1693(00)90134-8

Reference yield:

: sodium tetrachloropalladate(II)

: 35684-37-8
bis(4-methoxyphenyl)ditelluride

: 119053-80-4
{PdCl(TeC₆H₄OCH₃-4)}

Guidance literature:: In ethanol; under N2, at 40°C or above; washed with water, alcohol and CHCl3, good yield, isolated pure;
DOI:10.1016/S0020-1693(00)90134-8

Reference yield: 58.0%

: 119053-80-4
{PdCl(TeC₆H₄OCH₃-4)}

: 119030-11-4,125950-08-5
trans-{PdCl(TeC₆H₄OCH₃-4)(PPh₃)2}

Guidance literature:: With triphenylphosphine; In dichloromethane; under N2, excess PPh3, stirred for 6 h; concd., treated with petroleum ether, solid washed with petroleum ether and diethyl ether, dried in vac.; elem. anal.;
DOI:10.1016/S0020-1693(00)90134-8