ethyl 3-fluoro-4-(trifluoromethyl)benzenecarboximidoate hydrochloride

Base Information

Chemical Name:ethyl 3-fluoro-4-(trifluoromethyl)benzenecarboximidoate hydrochloride
CAS No.:1345003-71-5
Molecular Formula:C₁₀H₉F₄NO*ClH
Molecular Weight:271.642
Hs Code.:

Synonyms:

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Chemical Property of ethyl 3-fluoro-4-(trifluoromethyl)benzenecarboximidoate hydrochloride

Chemical Property:

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Technology Process of ethyl 3-fluoro-4-(trifluoromethyl)benzenecarboximidoate hydrochloride

There total 2 articles about ethyl 3-fluoro-4-(trifluoromethyl)benzenecarboximidoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115754-21-7
3-fluoro-4-(trifluoromethyl)benzoic acid

: 1345003-71-5
ethyl 3-fluoro-4-(trifluoromethyl)benzenecarboximidoate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 0 - 20 °C

1.2: 2 h / 0 - 20 °C

2.1: phosphorus pentachloride / pyridine / 2 h / Reflux

3.1: hydrogenchloride / diethyl ether / 76 h / 0 - 20 °C

With hydrogenchloride; oxalyl dichloride; phosphorus pentachloride; N,N-dimethyl-formamide; In pyridine; diethyl ether; dichloromethane;

Reference yield:

: 247170-27-0
3-fluoro-4-(trifluoromethyl)benzamide

: 1345003-71-5
ethyl 3-fluoro-4-(trifluoromethyl)benzenecarboximidoate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentachloride / pyridine / 2 h / Reflux

2: hydrogenchloride / diethyl ether / 76 h / 0 - 20 °C

With hydrogenchloride; phosphorus pentachloride; In pyridine; diethyl ether;

Reference yield:

: 1345003-71-5
ethyl 3-fluoro-4-(trifluoromethyl)benzenecarboximidoate hydrochloride

: 1345003-75-9
5-[3-fluoro-4-(trifluoromethyl)phenyl]-1,2,4-oxadiazol-3-amine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / 0 - 20 °C

2: hydroxylamine hydrochloride; triethylamine / ethanol / 0 - 20 °C

With hydroxylamine hydrochloride; triethylamine; In ethanol;