(diphenyl-p-tolylsilyl)tris(triphenylphosphane)silver(I)

Base Information

Chemical Name:(diphenyl-p-tolylsilyl)tris(triphenylphosphane)silver(I)
CAS No.:127915-35-9
Molecular Formula:C₇₃H₆₂AgP₃Si
Molecular Weight:1168.17
Hs Code.:

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Chemical Property of (diphenyl-p-tolylsilyl)tris(triphenylphosphane)silver(I)

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Technology Process of (diphenyl-p-tolylsilyl)tris(triphenylphosphane)silver(I)

There total 2 articles about (diphenyl-p-tolylsilyl)tris(triphenylphosphane)silver(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 124393-01-7
LiSi(C₆H₅)2(C₆H₄(CH₃))

: 54937-07-4
{AgI(triphenylphosphine)}4

: 127915-35-9
(diphenyl-p-tolylsilyl)tris(triphenylphosphane)silver(I)

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; byproducts: LiCl; dropwise addn. of LiSiPhTol soln. to AgCl complex soln. in THF at -78°C; addn. of PPh3 soln.; stirring, -78°C, 30 min; heating to room temp.; evapn. in high vac.; all operations under N2 excluding light; digerating with ether; filtration over Al2O3-silica gel (2:1); evapn.; dissoln. in a minimum amt. of petroleum ether; pptn. at -25°C; drying in high vac.; elem anal.; all operations excluding light;

Reference yield: 19.0%

: 124393-01-7
LiSi(C₆H₅)2(C₆H₄(CH₃))

: silver(I) chloride

: 127915-35-9
(diphenyl-p-tolylsilyl)tris(triphenylphosphane)silver(I)

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; byproducts: LiCl; addn. of LiSiPhTol soln. to suspn. of freshly pptd. AgCl in THF at -78°C; addn. of PPh3 soln.; vigorously stirring, 60 min; heating to room temp.; evapn. in high vac.; all operations under N2 excluding light; digerating with ether; filtration over Al2O3-silica gel (2:1); evapn.; dissoln. in a minimum amt. of petroleum ether; pptn. at -25°C; drying in high vac.; elem anal.; all operations excluding light;