Technology Process of C32H36N4O4
There total 6 articles about C32H36N4O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C32H38N4O5;
With
diethylamine;
In
dichloromethane;
at 20 ℃;
for 5h;
In
ethanol;
for 24h;
Reflux;
DOI:10.1016/j.bmcl.2012.11.011
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triphenylphosphine; 1,1,1,3,3,3-hexachloro-propan-2-one / dichloromethane / 0.58 h / -10 - 20 °C
2.1: tetrakis(triphenylphosphine) palladium(0) / toluene / 1 h / Reflux
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
4.1: ethanol / 24 h / Reflux
5.1: palladium 10% on activated carbon; cyclohexa-1,4-diene / ethanol / 24 h / Reflux
6.1: diethylamine / dichloromethane / 5 h / 20 °C
6.2: 24 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); 1,1,1,3,3,3-hexachloro-propan-2-one; cyclohexa-1,4-diene; palladium 10% on activated carbon; diethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine;
In
ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2012.11.011
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium 10% on activated carbon; cyclohexa-1,4-diene / ethanol / 24 h / Reflux
2.1: diethylamine / dichloromethane / 5 h / 20 °C
2.2: 24 h / Reflux
With
cyclohexa-1,4-diene; palladium 10% on activated carbon; diethylamine;
In
ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.011
