(R)-(-)-[1D₁]-S-benzyl O,O-diisopropyl thiophosphate

Base Information

Chemical Name:(R)-(-)-[1D₁]-S-benzyl O,O-diisopropyl thiophosphate
CAS No.:1315562-87-8
Molecular Formula:C₁₃H₂₁O₃PS
Molecular Weight:289.34
Hs Code.:

(R)-(-)-[1D<sub>1</sub>]-S-benzyl O,O-diisopropyl thiophosphate

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Chemical Property of (R)-(-)-[1D₁]-S-benzyl O,O-diisopropyl thiophosphate

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Technology Process of (R)-(-)-[1D₁]-S-benzyl O,O-diisopropyl thiophosphate

There total 3 articles about (R)-(-)-[1D₁]-S-benzyl O,O-diisopropyl thiophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1315562-87-8
(R)-(-)-[1D₁]-S-benzyl O,O-diisopropyl thiophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 °C / Inert atmosphere

1.2: 5 h / -78 - -10 °C / Inert atmosphere

2.1: isopropyl alcohol / 1 h / Reflux

With n-butyllithium; In tetrahydrofuran; hexane; isopropyl alcohol;
DOI:10.1039/c1ob05246b

Reference yield:

: 1809-20-7
diisopropyl hydrogenphosphonate

: 1315562-87-8
(R)-(-)-[1D₁]-S-benzyl O,O-diisopropyl thiophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfur / isopropyl alcohol / 2 h / 50 °C

2: isopropyl alcohol / 1 h / Reflux

With sulfur; In isopropyl alcohol;
DOI:10.1039/c1ob05246b