4-Morpholinecarbothioic acid, O-(pentachlorophenyl) ester

Base Information

• Chemical Name: 4-Morpholinecarbothioic acid, O-(pentachlorophenyl) ester
• CAS No.: 100991-59-1
• Molecular Formula: C₁₁H₈Cl₅NO₂S
• Molecular Weight: 395.521
• Mol file: 100991-59-1.mol

Synonyms:

Chemical Property of 4-Morpholinecarbothioic acid, O-(pentachlorophenyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Morpholinecarbothioic acid, O-(pentachlorophenyl) ester

There total 2 articles about 4-Morpholinecarbothioic acid, O-(pentachlorophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

morpholine (110-91-8,99108-56-2) + C9H3Cl7O2S2 (99498-87-0) → Morpholine-4-carbothioic acid O-pentachlorophenyl ester (100991-59-1)

Guidance literature:

In diethyl ether;

DOI:10.1016/S0040-4020(01)87479-2

Reference yield:

C7Cl8OS (99498-86-9) → Morpholine-4-carbothioic acid O-pentachlorophenyl ester (100991-59-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / CCl₄ / 50 - 60 °C

2: 71 percent / diethyl ether

In tetrachloromethane; diethyl ether;

DOI:10.1016/S0040-4020(01)87479-2

upstream raw materials:

morpholine

C₉H₃Cl₇O₂S₂

C₇Cl₈OS

Refernces