C₄₀H₃₃P

Base Information

Chemical Name:C₄₀H₃₃P
CAS No.:1393478-62-0
Molecular Formula:C₄₀H₃₃P
Molecular Weight:544.676
Hs Code.:

Synonyms:

Suppliers and Price of C₄₀H₃₃P

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₀H₃₃P

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₀H₃₃P

There total 4 articles about C₄₀H₃₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10-phenyl-5,6-dipropyl-10H-naphtho[1',2':5,6]phenanthro[3,4-f]phosphindole 10-oxide

: 1393478-62-0,1393478-63-1
C₄₀H₃₃P

Guidance literature:: With trichlorosilane; triethylamine; In toluene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201202024

Reference yield:

: 1393367-81-1
5-hydroxy-1-phenyl-1H-phosphindole 1-oxide

: 1393478-62-0,1393478-63-1
C₄₀H₃₃P

Guidance literature:: Multi-step reaction with 5 steps

1: caesium carbonate / N,N-dimethyl-formamide / 18 h / Inert atmosphere

2: PdCl₂(SPhos)2; caesium carbonate / tetrahydrofuran; water / 4 h / 85 °C

3: iodine; methyloxirane / tetrahydrofuran; cyclohexane / 17 h / Inert atmosphere; UV-irradiation

4: chiral SFC AD-H column / ethanol / 40 °C / 112511 Torr

5: trichlorosilane; triethylamine / toluene / 1 h / 20 °C / Inert atmosphere

With PdCl₂(SPhos)2; trichlorosilane; iodine; caesium carbonate; triethylamine; methyloxirane; In tetrahydrofuran; ethanol; cyclohexane; water; N,N-dimethyl-formamide; toluene; 2: Suzuki coupling;
DOI:10.1002/anie.201202024

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 1393478-62-0,1393478-63-1
C₄₀H₃₃P

Guidance literature:: Multi-step reaction with 8 steps

1.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.17 h / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / dichloromethane / 0.5 h / Inert atmosphere

4.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / Inert atmosphere

5.1: PdCl₂(SPhos)2; caesium carbonate / tetrahydrofuran; water / 4 h / 85 °C

6.1: iodine; methyloxirane / tetrahydrofuran; cyclohexane / 17 h / Inert atmosphere; UV-irradiation

7.1: chiral SFC AD-H column / ethanol / 40 °C / 112511 Torr

8.1: trichlorosilane; triethylamine / toluene / 1 h / 20 °C / Inert atmosphere

With PdCl₂(SPhos)2; trichlorosilane; tetrabutyl ammonium fluoride; iodine; tert.-butyl lithium; caesium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; methyloxirane; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; toluene; pentane; 5.1: Suzuki coupling;
DOI:10.1002/anie.201202024