Technology Process of C46H32N2O2
There total 6 articles about C46H32N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 36h;
Inert atmosphere;
DOI:10.1002/anie.201108610
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 36h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetra-N-butylammonium tribromide / methanol; dichloromethane / 1 h / 20 °C
2: pyridine
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; toluene / 48 h / Inert atmosphere; Reflux
4: water; potassium hydroxide
5: potassium carbonate / N,N-dimethyl-formamide / 36 h / 100 °C / Inert atmosphere
With
pyridine; tetrakis(triphenylphosphine) palladium(0); water; tetra-N-butylammonium tribromide; sodium carbonate; potassium carbonate; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201108610