Technology Process of C41H37F9N4O2
There total 5 articles about C41H37F9N4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tetrahydrofuran;
at 0 - 20 ℃;
for 12h;
Inert atmosphere;
Darkness;
DOI:10.1039/c0nj00264j
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / dimethyl sulfoxide / 100 °C
2: tetrahydrofuran / 15 h / 0 - 20 °C / Inert atmosphere; Darkness
3: dimethyl sulfoxide / 33 h / Alkaline conditions; Darkness; Heating
4: dimethyl sulfoxide / 20 h / Alkaline conditions; Darkness; Heating
5: tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere; Darkness
With
potassium carbonate;
In
tetrahydrofuran; dimethyl sulfoxide;
2: Wittig reaction;
DOI:10.1039/c0nj00264j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dimethyl sulfoxide / 33 h / Alkaline conditions; Darkness; Heating
2: dimethyl sulfoxide / 20 h / Alkaline conditions; Darkness; Heating
3: tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere; Darkness
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1039/c0nj00264j