Technology Process of C20H24N2O11S2
There total 9 articles about C20H24N2O11S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: sodium hydride / N,N-dimethyl-formamide
2: water; acetic acid
3: sodium periodate
4: sodium hydroxide
6: sulfuric acid; acetic acid
7: trimethylsilyl trifluoromethanesulfonate; BSA
8: methanol; ammonia
9: oxalyl dichloride; dimethyl sulfoxide; triethylamine
With
methanol; sodium periodate; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; ammonia; water; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; BSA;
In
N,N-dimethyl-formamide;
7: Vorbruggen reaction / 9: Swern oxidation;
DOI:10.1016/j.bmcl.2011.06.104
- Guidance literature:
-
Multi-step reaction with 10 steps
1: lithium triethylborohydride / dichloromethane
2: sodium hydride / N,N-dimethyl-formamide
3: water; acetic acid
4: sodium periodate
5: sodium hydroxide
7: sulfuric acid; acetic acid
8: trimethylsilyl trifluoromethanesulfonate; BSA
9: methanol; ammonia
10: oxalyl dichloride; dimethyl sulfoxide; triethylamine
With
methanol; sodium periodate; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; ammonia; water; sodium hydride; lithium triethylborohydride; acetic acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; BSA;
In
dichloromethane; N,N-dimethyl-formamide;
8: Vorbruggen reaction / 10: Swern oxidation;
DOI:10.1016/j.bmcl.2011.06.104