β-Hydroxy-β--propionsaeure-anilid

Base Information

• Chemical Name: β-Hydroxy-β--propionsaeure-anilid
• CAS No.: 93008-71-0
• Molecular Formula: C₁₆H₁₇NO₂
• Molecular Weight: 255.316

Synonyms:

Chemical Property of β-Hydroxy-β--propionsaeure-anilid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of β-Hydroxy-β--propionsaeure-anilid

There total 2 articles about β-Hydroxy-β--propionsaeure-anilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-ethenyl-4-methylbenzene (622-97-9,24936-41-2) → β-Hydroxy-β--propionsaeure-anilid (93008-71-0)

Guidance literature:

Multi-step reaction with 2 steps

2: diethyl ether / 336 h / Ambient temperature

In diethyl ether;

Reference yield:

1-Hydroxy-3-trichloracetyloxy-3-(4-methyl-phenyl)-1,1-dicyano-propan (96775-25-6) + aniline (62-53-3) → β-Hydroxy-β--propionsaeure-anilid (93008-71-0)

Guidance literature:

In diethyl ether; for 336h; Ambient temperature;

Reference yield:

β-Hydroxy-β--propionsaeure-anilid (93008-71-0) → p-methyl-N-phenylcinnamamide (15795-11-6,365410-94-2)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; Heating;

upstream raw materials:

1-Hydroxy-3-trichloracetyloxy-3-(4-methyl-phenyl)-1,1-dicyano-propan

aniline

1-ethenyl-4-methylbenzene

Downstream raw materials:

p-methyl-N-phenylcinnamamide

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