2-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)maleimide

Base Information

Chemical Name:2-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)maleimide
CAS No.:79934-04-6
Molecular Formula:C₃₀H₂₉NO₆
Molecular Weight:499.563
Hs Code.:

Synonyms:

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Chemical Property of 2-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)maleimide

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Technology Process of 2-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)maleimide

There total 6 articles about 2-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)maleimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54656-61-0
2,3,5-tri-O-benzyl-α-D-ribofuranosylethyne

: 79934-04-6
2-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)maleimide

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / mercury⁽¹¹⁾ chloride / palladium chloride / 21 h / 1520 Torr / Ambient temperature

2: 100 percent / potassium hydroxide / dioxane; H₂O / 24 h

3: 1.31 g / acetic anhydride / 20 h / Ambient temperature

4: 1.) ammonia, 2.) acetyl chloride / 1.) 0 deg C, 10 min, 2.) DMF, RT, 20 h

With potassium hydroxide; ammonia; acetic anhydride; acetyl chloride; mercury dichloride; palladium dichloride; In 1,4-dioxane; water;
DOI:10.1039/P19810002267

Reference yield:

: 79875-99-3
(2R,3R,4R)-2,3,4,5-tetrakis(benzyloxy)pentanal

: 79934-04-6
2-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)maleimide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) magnesium, ethyl bromide / 1.) THF, 2.) THF, 1 h, 3.) THF, 2 h

2: 42 percent / toluene-p-sulphonyl chloride / pyridine / Ambient temperature

3: 65 percent / mercury⁽¹¹⁾ chloride / palladium chloride / 21 h / 1520 Torr / Ambient temperature

4: 100 percent / potassium hydroxide / dioxane; H₂O / 24 h

5: 1.31 g / acetic anhydride / 20 h / Ambient temperature

6: 1.) ammonia, 2.) acetyl chloride / 1.) 0 deg C, 10 min, 2.) DMF, RT, 20 h

With potassium hydroxide; ethyl bromide; ammonia; acetic anhydride; magnesium; acetyl chloride; p-toluenesulfonyl chloride; mercury dichloride; palladium dichloride; In 1,4-dioxane; pyridine; water;
DOI:10.1039/P19810002267

Reference yield:

: (4S,5R,6R)-4,5,6,7-Tetrakis-benzyloxy-hept-1-yn-3-ol

: 79934-04-6
2-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)maleimide

Guidance literature:: Multi-step reaction with 5 steps

1: 42 percent / toluene-p-sulphonyl chloride / pyridine / Ambient temperature

2: 65 percent / mercury⁽¹¹⁾ chloride / palladium chloride / 21 h / 1520 Torr / Ambient temperature

3: 100 percent / potassium hydroxide / dioxane; H₂O / 24 h

4: 1.31 g / acetic anhydride / 20 h / Ambient temperature

5: 1.) ammonia, 2.) acetyl chloride / 1.) 0 deg C, 10 min, 2.) DMF, RT, 20 h

With potassium hydroxide; ammonia; acetic anhydride; acetyl chloride; p-toluenesulfonyl chloride; mercury dichloride; palladium dichloride; In 1,4-dioxane; pyridine; water;
DOI:10.1039/P19810002267