sulfure de dimethyl-1,1 diphenylphosphino-3 butane

Base Information

Chemical Name:sulfure de dimethyl-1,1 diphenylphosphino-3 butane
CAS No.:82364-05-4
Molecular Formula:C₁₈H₂₃PS
Molecular Weight:302.42
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sulfure de dimethyl-1,1 diphenylphosphino-3 butane

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Technology Process of sulfure de dimethyl-1,1 diphenylphosphino-3 butane

There total 4 articles about sulfure de dimethyl-1,1 diphenylphosphino-3 butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3190-79-2
(2-mercaptoethyl)diphenylphosphine

: 82364-05-4
sulfure de dimethyl-1,1 diphenylphosphino-3 butane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / S₈ / benzene / Ambient temperature

2: 1.) TMEDA; 2.) HCl / 1.) hexane, benzene, -40 deg C, 1 h; 2.) H₂O, RT

With hydrogenchloride; sulfur; N,N,N,N,-tetramethylethylenediamine; In benzene;
DOI:10.1139/v82-126

Reference yield:

: 82364-10-1
sulfure de diphenylphosphino-2 ethanethiol

: 82364-05-4
sulfure de dimethyl-1,1 diphenylphosphino-3 butane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 1 h, RT; 2.) THF, 1 h, RT

2: 1.) TMEDA; 2.) 3N HCl / 1.) hexane, benzene, -40 deg C, 1 h

With hydrogenchloride; N,N,N,N,-tetramethylethylenediamine; sodium hydride;
DOI:10.1139/v82-126

Reference yield:

: 594-19-4
tert.-butyl lithium

: 82364-10-1
sulfure de diphenylphosphino-2 ethanethiol

: 82364-05-4
sulfure de dimethyl-1,1 diphenylphosphino-3 butane

Guidance literature:: With hydrogenchloride; N,N,N,N,-tetramethylethylenediamine; Yield given. Multistep reaction; 1.) hexane, benzene, -40 deg C, 1 h; 2.) H₂O, RT;
DOI:10.1139/v82-126