trans-1-Benzyl-4-<3--2-oxopropyl>-2-piperidinocarbonitrile

Base Information

Chemical Name:trans-1-Benzyl-4-<3--2-oxopropyl>-2-piperidinocarbonitrile
CAS No.:135634-84-3
Molecular Formula:C₃₁H₃₃N₃O₂
Molecular Weight:479.622
Hs Code.:

trans-1-Benzyl-4-<3-<o-(N-benzylacetamido)phenyl>-2-oxopropyl>-2-piperidinocarbonitrile

Synonyms:

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Chemical Property of trans-1-Benzyl-4-<3--2-oxopropyl>-2-piperidinocarbonitrile

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Technology Process of trans-1-Benzyl-4-<3--2-oxopropyl>-2-piperidinocarbonitrile

There total 6 articles about trans-1-Benzyl-4-<3--2-oxopropyl>-2-piperidinocarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116787-78-1
1-(1-benzyl-4-piperydyl)-3-(o-nitrophenyl)-2-propanone

: 135634-84-3
trans-1-Benzyl-4-<3--2-oxopropyl>-2-piperidinocarbonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / p-TsOH*H₂O / benzene / 24 h / Heating

2: 65 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr

3: 58 percent / ethanol / 15 h / Heating

4: 2) 12N HCl / 1) 5 h, r.t. 2) water, 45 min

With hydrogenchloride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)87110-6

Reference yield:

: 135634-74-1
1-Benzyl-4-<2,2-(ethylenedioxy)-3-(o-nitrophenyl)propyl>piperidine

: 135634-84-3
trans-1-Benzyl-4-<3--2-oxopropyl>-2-piperidinocarbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / H₂ / 10percent Pd/C / ethanol / 760 Torr

2: 58 percent / ethanol / 15 h / Heating

3: 2) 12N HCl / 1) 5 h, r.t. 2) water, 45 min

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4020(01)87110-6

Reference yield:

: 100-44-7
benzyl chloride

: 135634-84-3
trans-1-Benzyl-4-<3--2-oxopropyl>-2-piperidinocarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / ethanol / 15 h / Heating

2: 2) 12N HCl / 1) 5 h, r.t. 2) water, 45 min

With hydrogenchloride; In ethanol;
DOI:10.1016/S0040-4020(01)87110-6