(+/-)-O-methylorantine

Base Information

Chemical Name:(+/-)-O-methylorantine
CAS No.:64366-67-2
Molecular Formula:C₂₉H₃₈N₄O₄
Molecular Weight:506.645
Hs Code.:

Synonyms:

Suppliers and Price of (+/-)-O-methylorantine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-O-methylorantine

Chemical Property:

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Technology Process of (+/-)-O-methylorantine

There total 13 articles about (+/-)-O-methylorantine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94405-69-3,94481-31-9
C₃₄H₄₆N₄O₆

: 64366-67-2,69721-60-4,94481-32-0,94481-33-1
(+/-)-O-methylorantine

Guidance literature:: With hydrogenchloride; In dichloromethane; at -10 - 0 ℃; Yield given;
DOI:10.1021/ja00288a050

Reference yield:

: 3943-97-3
methyl 4-hydroxycinnamate

: 64366-67-2,69721-60-4,94481-32-0,94481-33-1
(+/-)-O-methylorantine

Guidance literature:: Multi-step reaction with 11 steps

1: 57 percent / potassium ferricyanide/Na₂CO₃ / H₂O; CHCl₃

2: 74 percent / acetone / 25 °C

3: NaN₃/ICl / acetonitrile / 0 °C

4: tributyltin hydride / benzene / 20 h / 25 °C

5: 32 percent / chlorobenzene / 9 h / 132 °C

6: 90 percent / NaBH₃CN / acetic acid / 1.) 25 deg C, 2 h; 2.) 50 deg C, 1 h; 3.) 25 deg C, 12 h

7: barium hydroxide / tetrahydrofuran; methanol

8: DCC

9: powdered zinc/acetic acid

10: 17 percent / N,N-diisopropylethylamine/1-hydroxybenzotriazole / dimethylformamide / 10 h / 40 °C

11: HCl / CH₂Cl₂ / -10 - 0 °C

With hydrogenchloride; barium dihydroxide; sodium azide; tri-n-butyl-tin hydride; Iodine monochloride; sodium cyanoborohydride; sodium carbonate; benzotriazol-1-ol; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; potassium hexacyanoferrate(III); zinc; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; acetic acid; N,N-dimethyl-formamide; chlorobenzene; acetone; acetonitrile; benzene;
DOI:10.1021/ja00288a050

Reference yield:

: 84877-90-7
(E)-4-Methoxy-1,5,9-triaza-cyclotridec-4-ene-1,9-dicarboxylic acid 1-tert-butyl ester 9-(2,2,2-trichloro-ethyl) ester

: 64366-67-2,69721-60-4,94481-32-0,94481-33-1
(+/-)-O-methylorantine

Guidance literature:: Multi-step reaction with 7 steps

1: 32 percent / chlorobenzene / 9 h / 132 °C

2: 90 percent / NaBH₃CN / acetic acid / 1.) 25 deg C, 2 h; 2.) 50 deg C, 1 h; 3.) 25 deg C, 12 h

3: barium hydroxide / tetrahydrofuran; methanol

4: DCC

5: powdered zinc/acetic acid

6: 17 percent / N,N-diisopropylethylamine/1-hydroxybenzotriazole / dimethylformamide / 10 h / 40 °C

7: HCl / CH₂Cl₂ / -10 - 0 °C

With hydrogenchloride; barium dihydroxide; sodium cyanoborohydride; benzotriazol-1-ol; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; zinc; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1021/ja00288a050