Technology Process of 1-
-3,5-diphenylcyclohexane
There total 6 articles about 1--3,5-diphenylcyclohexane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 88 percent / diethyl ether / 1) 1h, RT, 2) 4h, reflux
2: 55 percent / p-TsOH / benzene / 4 h / Heating
3: 86 percent / pyridine hydrochloride / 220 °C
4: 100 percent / H2 / 10percent Pd-C / methanol
5: 74 percent / K2CO3 / acetone / 15 h / Heating
6: 82 percent / K2CO3 / acetone / 24 h / Heating
With
hydrogen; pyridine hydrochloride; potassium carbonate; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
methanol; diethyl ether; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / H2 / 10percent Pd-C / methanol
2: 74 percent / K2CO3 / acetone / 15 h / Heating
3: 82 percent / K2CO3 / acetone / 24 h / Heating
With
hydrogen; potassium carbonate;
palladium on activated charcoal;
In
methanol; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 86 percent / pyridine hydrochloride / 220 °C
2: 100 percent / H2 / 10percent Pd-C / methanol
3: 74 percent / K2CO3 / acetone / 15 h / Heating
4: 82 percent / K2CO3 / acetone / 24 h / Heating
With
hydrogen; pyridine hydrochloride; potassium carbonate;
palladium on activated charcoal;
In
methanol; acetone;
